5-[(E)-丙-1-烯基]苯并[1,3]二氧杂环戊烯合成路线 （共 45 条）
反应条件
1: N-bromosuccinimide / dimethylsulfoxide; H2O 2: 75 percent / K2CO3 / Pd(OAc)2, P(o-Tol)3 / benzene / 5 h / 100 °C View Scheme
参考文献
Tsuji, Jiro; Nagashima, Hideo; Sato, Koji
Tetrahedron Letters, 1982 , vol. 23, # 30 p. 3085 - 3088
反应条件
sodium hydroxide; formic acid; sulfuric acid; dihydrogen peroxide in methanol; water; acetone
参考文献
Microgenics Corporation
Patent: US2003/207469 A1, 2003 ;
反应条件
oxygen; copper(l) chloride; palladium dichloride in water; N,N-dimethyl-formamide T=50°C; 10 h;
参考文献
Nagashima, Hideo; Sato, Koji; Tsuji, Jiro
Tetrahedron, 1985 , vol. 41, # 23 p. 5645 - 5652
反应条件
1: 11 percent / m-CPBA / CH2Cl2 / 0.5 h / 0 °C 2: 69 percent / BF3*OEt2 / 0.33 h / Ambient temperature View Scheme
参考文献
Nagashima, Hideo; Sato, Koji; Tsuji, Jiro
Tetrahedron, 1985 , vol. 41, # 23 p. 5645 - 5652
反应条件
resine C35O; hydrogen cation in benzene T=60°C; 12 h;
参考文献
Delmas, Michel; Gaset, Antoine
Tetrahedron Letters, 1981 , vol. 22, p. 723 - 724
反应条件
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 0.42 h / Heating; Microwave irradiation 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 0.5 h / Heating; Microwave irradiation View Scheme
参考文献
Sharma, Abhishek; Sharma, Naina; Shard, Amit; Kumar, Rakesh; Mohanakrishnan, Dinesh; Saima; Sinha, Arun K.; Sahal, Dinkar
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 14 p. 5211 - 5219
反应条件
methyl 1-naphthyl ketone; lithium perchlorate; acetic acid 1) MeCN, 17 h, irradiation, 2) MeCN, anodic oxidation, 24-28 deg C; Yield given. Multistep reaction;
参考文献
Gates, Bradley D.; Swenton, John S.
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2127 - 2128
反应条件
potassium hydroxide in butan-1-ol
3 h; Ambient temperature;
参考文献
Gauthier, Delphine; Lindhardt, Anders T.; Olsen, Esben P. K.; Overgaard, Jacob; Skrydstrup, Troels
Journal of the American Chemical Society, 2010 , vol. 132, # 23 p. 7998 - 8009
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether
T=30°C;
参考文献
Rossi, Renzo; Carpita, Adriano
Tetrahedron Letters, 1986 , vol. 27, # 22 p. 2529 - 2532
反应条件
silica gel; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane
T=20°C;
参考文献
Joshi, Bhupendra P.; Sharma, Anuj; Sinha, Arun K.
Tetrahedron, 2005 , vol. 61, # 12 p. 3075 - 3080
