1-乙酰基-3,5-二甲基金刚烷合成路线 (共 4 条)
反应条件
1: in diethyl ether
T=0 - 20°C; 4.5 h; Inert atmosphere;
2: With hydrogenchloride in diethyl ether; water
Inert atmosphereCooling with ice;
参考文献
Tsubo, Tatsuyuki; Chen, Hsiu-Hui; Yokomori, Minako; Fukui, Kosuke; Kikuchi, Satoshi; Yamada, Tohru
Chemistry Letters, 2012 , vol. 41, # 8 p. 780 - 782
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6429314 B1, 2002 ;
反应条件
1.1: Jone's reagent / Inert atmosphere
2.1: diethyl ether / 4.5 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere; Cooling with ice
View Scheme
参考文献
Tsubo, Tatsuyuki; Chen, Hsiu-Hui; Yokomori, Minako; Fukui, Kosuke; Kikuchi, Satoshi; Yamada, Tohru
Chemistry Letters, 2012 , vol. 41, # 8 p. 780 - 782
反应条件
in dichloromethane
Irradiation;
参考文献
Tabushi,I. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 12 p. 2370 - 2374