(Z)-十二碳-5-烯醇合成路线 （共 25 条）
反应条件
1: KOH / ethane-1,2-diol / 6 h / Heating
3: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature
View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
1: LiBr / acetone / 5 h / Ambient temperature
2: 73 percent / dimethylsulfoxide / Ambient temperature
3: KOH / ethane-1,2-diol / 6 h / Heating
5: lithium aluminium hydride / diethyl ether / 3 h / Ambient temperature
View Scheme
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
反应条件
sodium amide
1.) THF, 25 deg C, 30 min, 2.) -80 deg C to 25 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Schaub, Bruno; Blaser, Gottfried; Schlosser, M.
Tetrahedron Letters, 1985 , vol. 26, # 3 p. 307 - 310
反应条件
pyridine in benzene
T=20°C;
参考文献
Kovalev, B. G.; Dzhumakulov, T.; Abduvakhabov, A. A.; Sadykov, A. S.
Doklady Chemistry, 1987 , vol. 297, # 12 p. 544 - 548
Dokl. Akad. Nauk SSSR Ser. Khim., 1987 , vol. 297, # 6 p. 1381 - 1386
反应条件
pyridine
24 h; Ambient temperature;
参考文献
Kelkar, S. V.; Reddy, G. Bhaskar; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 980 - 981
