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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
40646-17-1
合成路线
（共 20 条）
40646-17-1
→
反应条件
764-89-6
8-羟基辛酸
反应条件
1: PDC View Scheme
参考文献
Plettner; Sutherland; Slessor; Winston
Journal of Chemical Ecology, 1995 , vol. 21, # 7 p. 1017 - 1029
40646-17-1
→
反应条件
35153-20-9
(12Z)-12-十四碳烯-1-基乙酸酯
反应条件
1.1: pyridinium chlorochromate / dichloromethane / 20 °C 2.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere 2.2: -15 - 20 °C / Inert atmosphere 3.1: nitric acid; sodium nitrite / water / 1 h / 70 - 75 °C / Inert atmosphere View Scheme
参考文献
Li, Jiu-Ming; Yong, Jian-Ping; Huang, Feng-Lan; Bai, Shu-Zhen
Chemistry of Natural Compounds, 2012 , vol. 48, # 1 p. 103 - 105
40646-17-1
→
反应条件
35153-20-9
(12Z)-12-十四碳烯-1-基乙酸酯
反应条件
1.1: pyridinium chlorochromate / dichloromethane / 20 °C 2.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere 2.2: -15 - 20 °C / Inert atmosphere View Scheme
参考文献
Li, Jiu-Ming; Yong, Jian-Ping; Huang, Feng-Lan; Bai, Shu-Zhen
Chemistry of Natural Compounds, 2012 , vol. 48, # 1 p. 103 - 105
40646-17-1
→
反应条件
35153-20-9
(12Z)-12-十四碳烯-1-基乙酸酯
反应条件
1.1: pyridinium chlorochromate / dichloromethane / 20 °C 2.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere 2.2: -15 - 20 °C / Inert atmosphere 3.1: nitric acid; sodium nitrite / water / 1 h / 70 - 75 °C / Inert atmosphere View Scheme
参考文献
Li, Jiu-Ming; Yong, Jian-Ping; Huang, Feng-Lan; Bai, Shu-Zhen
Chemistry of Natural Compounds, 2012 , vol. 48, # 1 p. 103 - 105
40646-17-1
→
反应条件
35153-20-9
(12Z)-12-十四碳烯-1-基乙酸酯
反应条件
1.1: pyridinium chlorochromate / dichloromethane / 20 °C 2.1: potassium tert-butylate / tetrahydrofuran / Inert atmosphere 2.2: -15 - 20 °C / Inert atmosphere View Scheme
参考文献
Li, Jiu-Ming; Yong, Jian-Ping; Huang, Feng-Lan; Bai, Shu-Zhen
Chemistry of Natural Compounds, 2012 , vol. 48, # 1 p. 103 - 105
1403675-04-6
→
反应条件
40646-17-1
反应条件
Pd(OH)2/C in isopropyl alcohol 1.5 h; Reflux;
参考文献
Mart, Alson; Shashidhar, Mysore S.
Tetrahedron, 2012 , vol. 68, # 47 p. 9769 - 9776,8
Title/Abstract Full Text Show Details
Mart, Alson; Shashidhar, Mysore S.
Tetrahedron, 2012 , vol. 68, # 47 p. 9769 - 9776
629-41-4
1,8-辛二醇
+
64-19-7
醋酸
→
反应条件
40646-17-1
反应条件
HY-Zeolite in chloroform 3.5 h; Heating;
参考文献
Srinivas; Mahender; Das, Biswanath
Synlett, 2003 , # 15 p. 2419 - 2421
3992-48-1
1,8-二乙酰氧基辛烷
→
反应条件
40646-17-1
反应条件
HY-Zeolite in methanol 4 h; Heating;
参考文献
Srinivas; Mahender; Das, Biswanath
Synlett, 2003 , # 15 p. 2419 - 2421
5048-35-1
乙酸-7-辛烯-1-基酯
→
反应条件
40646-17-1
反应条件
1: With 9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran T=0 - 10°C; 2: With dihydrogen peroxide; sodium acetate in tetrahydrofuran T=20°C; 2 h; Further stages.;
参考文献
Ishmuratov; Yakovleva; Tambovtsev; Legostaeva; Kravchenko; Ishmuratova; Tolstikov
Chemistry of Natural Compounds, 2008 , vol. 44, # 1 p. 74 - 76
108-05-4
醋酸乙烯酯
+
629-41-4
1,8-辛二醇
→
反应条件
3992-48-1
1,8-二乙酰氧基辛烷
+
40646-17-1
反应条件
Thermomyces lanuginosus lipase in di-isopropyl ether T=25°C;
参考文献
Framis, Victoria; Camps, Francisco; Clapes, Pere
Tetrahedron Letters, 2004 , vol. 45, # 26 p. 5031 - 5033
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