2-亚甲基环己烷-1-醇合成路线 （共 70 条）
反应条件
triethylaluminum in tetrahydrofuran
T=40°C;
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193
反应条件
triethylaluminum in tetrahydrofuran
T=40°C;
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193
反应条件
borane-THF in tetrahydrofuran
T=0°C; 1 h;
参考文献
Eid Jr.; Konopelski
Tetrahedron, 1991 , vol. 47, # 6 p. 975 - 992
反应条件
in tetrahydrofuran
T=25°C; 0.5 h;
参考文献
Ukai; Arioka; Yoshino; Fushimi; Oshima; Utimoto; Matsubara
Synlett, 2001 , # 4 p. 513 - 514
反应条件
1: MnO2, 20percent benzoquinone / 5percent Pd(OAc)2 / 24 h / 50 °C
2: 2M NaOH / methanol / 25 °C
View Scheme
参考文献
Hansson, Sverker; Heumann, Andreas; Rein, Tobias; Akermark, Bjoern
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 975 - 984
反应条件
1,3-dimethyl-imidazolidin-2-one; toluene-4-sulfonic acid in dichloromethane
T=20°C; 2 h; regioselective reaction;
参考文献
Chapman, Helen A.; Herbal, Karim; Motherwell, William B.
Synlett, 2010 , # 4 art. no. D37609ST, p. 595 - 598
反应条件
oxygen in acetonitrile
T=20°C; P=760.051 Torr; 24 h; UV-irradiation;
参考文献
Mori, Kohsuke; Kawashima, Masayoshi; Che, Michel; Yamashita, Hiromi
Angewandte Chemie - International Edition, 2010 , vol. 49, # 46 p. 8598 - 8601
反应条件
potassium hydroxide
DMSO, 110 deg C; Yield given. Multistep reaction;
参考文献
Trofimov, B. A.; Petrova, O. V.; Vasil'tsov, A. M.; Mikhaleva, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 7.2 p. 1450 - 1453
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 7 p. 1601 - 1605
反应条件
1: KOH / 110 deg C, 10 min
2: KOH / DMSO, 110 deg C
View Scheme
参考文献
Trofimov, B. A.; Petrova, O. V.; Vasil'tsov, A. M.; Mikhaleva, A. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 7.2 p. 1450 - 1453
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 7 p. 1601 - 1605
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1953 , vol. 75, p. 939,940
