2-亚甲基环己烷-1-醇合成路线 （共 70 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1953 , vol. 75, p. 939,940
反应条件
potassium tert-butylate
336 h; Ambient temperature;
参考文献
Goldmann, Siegfried
Synthesis, 1980 , # 8 p. 640 - 642
参考文献
Lessard,J. et al.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 1015 - 1023
反应条件
oxygen; 2(C4H9)4N(1+)*(Mo6Cl14)(2-)(excit.) in acetone
Irradiation;
参考文献
Jackson, Julie A.; Turro, Claudia; Newsham, Mark D.; Nocera, Daniel G.
Journal of Physical Chemistry, 1990 , vol. 94, # 11 p. 4500 - 4507
反应条件
potassium hydroxide
T=110°C;
参考文献
Trofimov, B. A.; Mikhaleva, A. I.; Petrova, O. V.; Sigalov, M. V.; Kalinina, N. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2211 - 2212
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2461 - 2462
反应条件
barium dihydroxide in water
T=90°C; further temperatures, enthalpy of reaction, entropy of reaction; Kinetics;
参考文献
Bartok, Mihaly; Felfoeldi, Karoly; Bozoki-Bartok, Gizella
Helvetica Chimica Acta, 1980 , vol. 63, # 8 p. 2173 - 2178
反应条件
selenium(IV) oxide; pinane hydroperoxide; acetic acid in dichloromethane; chlorobenzene
Ambient temperature; Yield given;
参考文献
Lempers; Ripolles i Garcia; Sheldon
Journal of Organic Chemistry, 1998 , vol. 63, # 5 p. 1408 - 1413
反应条件
toluene-4-sulfonic acid in dichloromethane
T=20°C; 2 h; regioselective reaction;
参考文献
Chapman, Helen A.; Herbal, Karim; Motherwell, William B.
Synlett, 2010 , # 4 art. no. D37609ST, p. 595 - 598
反应条件
1: m-CPBA / CH2Cl2
2: 88 percent / AlEt3 / tetrahydrofuran / 40 °C
View Scheme
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193
反应条件
1: m-CPBA / CH2Cl2
2: 89 percent / AlEt3 / tetrahydrofuran / 40 °C
View Scheme
参考文献
Wang, Fei; Wang, Shao Hua; Tu, Yong Qiang; Ren, Shi Kuo
Tetrahedron Asymmetry, 2003 , vol. 14, # 15 p. 2189 - 2193
