2-亚甲基环己烷-1-醇合成路线 （共 70 条）
参考文献
Chen, Yu-Zhe; Wu, Li-Zhu; Zhang, Li-Ping; Tung, Chen-Ho
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4676 - 4681
反应条件
potassium tert-butylate; water in dimethyl sulfoxide
T=100°C; 4 h;
参考文献
Trofimov, B. A.; Mikhaleva, A. I.; Petrova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 9.2 p. 1713 - 1718
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 9 p. 1941 - 1946
反应条件
potassium hydroxide
T=120°C; 1 h;
参考文献
Istomina, S. N.; Mikhaleva, A. I.; Petrova, O. V.; Trofimov, B. A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 3.1 p. 441 - 444
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 3 p. 516 - 520
反应条件
benzenethiol sodium salt
参考文献
Hannaby, Malcolm; Warren, Stuart
Tetrahedron Letters, 1985 , vol. 26, # 26 p. 3133 - 3136
反应条件
[(5,10,15,20-tetraphenylporphyrin)CrCl]; iodosylbenzene in dichloromethane
0.75 h; Ambient temperaturefurther reagents; MechanismProduct distribution;
参考文献
Groves, John T.; Subramanian, Durga V.
Journal of the American Chemical Society, 1984 , vol. 106, # 7 p. 2177 - 2181
反应条件
1: 1. Diisopropylamin, 15percent Butyllithium/Hexan / - 78 deg C, 10 min., THF
2: 72 percent / 1M tert-BuOK/tert-BuOK / 336 h / Ambient temperature
View Scheme
参考文献
Goldmann, Siegfried
Synthesis, 1980 , # 8 p. 640 - 642
反应条件
1: sodium periodate
2: 72 percent Spectr. / PhSNa
View Scheme
参考文献
Hannaby, Malcolm; Warren, Stuart
Tetrahedron Letters, 1985 , vol. 26, # 26 p. 3133 - 3136
反应条件
palladium diacetate; sodium hydroxide; trifluoroacetic acid; p-benozquinone
1.) acetic acid, room temperature, 118 h, 2.) methanol, 50 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Akermark, Bjoern; Hansson, Sverker; Rein, Tobias; Vagberg, Jan; Heumann, Andreas; Baeckvall, Jan-Erling
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 433 - 444
反应条件
pyridine; dihydrogen peroxide
参考文献
Clive,D.L.J. et al.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 770 - 771
反应条件
dimethylammonium chloride; potassium hydride; phosphorous acid trimethyl ester
1.) THF, 1 h, 0 deg C, 2.) CH3OH, 4 d, room temp.; Yield given. Multistep reaction;
参考文献
Hoffmann, Reinhard W.; Goldmann, Siegfried; Maak, Norbert; Gerlach, Rainer; Frickel, Fritz; Steinbach, Gertrud
Chemische Berichte, 1980 , vol. 113, # 3 p. 819 - 830
