([1-苯基-meth-(e)-基idene]-氨基)-乙酸 乙酯合成路线 （共 12 条）
反应条件
magnesium sulfate; triethylamine in dichloromethane T=20°C; 10 h;
参考文献
Gonzalez, Kelly A; Wilson, Lon J; Wu, Wenju; Nancollas, George H
Bioorganic and medicinal chemistry, 2002 , vol. 10, # 6 p. 1991 - 1997
反应条件
magnesium sulfate in dichloromethane T=20°C;
参考文献
Murugan, Ramalingam; Raghunathan; Narayanan, S. Sriman
Synthetic Communications, 2009 , vol. 39, # 11 p. 1936 - 1948
反应条件
1: 82 percent / dimethylsulfoxide / 2 h 2: NaH / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Unterhalt; Mohr
Archiv der Pharmazie, 1986 , vol. 319, # 5 p. 427 - 430
参考文献
Scheibler
Patent: DE386743 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1433
Full Text Show Details
Scheibler; Baumgarten
Chemische Berichte, 1922 , vol. 55, p. 1374
参考文献
Scheibler; Baumgarten
Chemische Berichte, 1922 , vol. 55, p. 1374
反应条件
1: 1) KOt-Bu / 1) THF, -78 deg C, 10 min, 2) THF, a) up to room temp., 1.5 h, b) room temp., 1.5 h 2: NaBH4 / ethanol / 15 h / Ambient temperature 3: 93 percent / AgBF4 / CH2Cl2 / 4 h / Ambient temperature 4: 1) ozone, 2) Me2S 5: LiAlH4 View Scheme
参考文献
Huby, Nicholas J. S.; Kinsman, Richard G.; Lathbury, David; Vernon, Peter G.; Gallagher, Timothy
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 145 - 155
反应条件
diethyl ether; aluminium amalgam; water
参考文献
Scheibler; Baumgarten
Chemische Berichte, 1922 , vol. 55, p. 1374
参考文献
Scheibler; Baumgarten
Chemische Berichte, 1922 , vol. 55, p. 1374
反应条件
sodium amalgam; water
参考文献
Scheibler; Baumgarten
Chemische Berichte, 1922 , vol. 55, p. 1374
反应条件
sodium hydride in diethyl ether; dimethyl sulfoxide
Ambient temperatureHeating1) r.t., 2) reflux, 30 min;
参考文献
Haddow, John; Suckling, Colin J.; Wood, Hamish C. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1297 - 1304
