反应条件
1.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.83 h / -78 °C 1.2: 58 percent / tetrahydrofuran / 1.5 h / -78 - 20 °C 2.1: pyridine; hydroxylamine hydrochloride / ethanol / 12 h / 60 °C 3.1: 99 percent / triethylamine / CH2Cl2 / 0.25 h / 0 °C 4.1: 28 percent / molecular sieves 4 Angstroem; t-Bu3P; triethylamine / bis(dibenzylideneacetone)palladium(0) / dimethylformamide; toluene / 0.5 h / 80 °C View Scheme
参考文献
Chiba, Shunsuke; Kitamura, Mitsuru; Saku, Osamu; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 4 p. 785 - 796
