1-氯-4-(4-甲氧基苯氧基)苯合成路线 （共 20 条）
参考文献
American Home Products Corporation
Patent: US5391571 A1, 1995 ;
US 5391571 A
反应条件
potassium carbonate in acetonitrile
T=50°C; 24 h; regioselective reaction;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium carbonate in acetonitrile
T=50°C; 24 h; Overall yield = 67 percent; regioselective reaction;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium carbonate in acetonitrile
T=50°C; 6 h; Overall yield = 91 percent; regioselective reaction;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
1: 2,2,2-trifluoroethanol
2: potassium carbonate / acetonitrile / 24 h / 50 °C
View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
1: iodine; dipotassium peroxodisulfate
2: potassium carbonate / acetonitrile / 30 h / 50 °C
View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
1: iodine; dipotassium peroxodisulfate
2: potassium carbonate / acetonitrile / 24 h / 50 °C
View Scheme
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
参考文献
Walter
Barell-Festschr. <Basel 1936> S. 266, 272, 273
反应条件
Yield given. Multistep reaction;
参考文献
Pearson, Anthony J.; Gelormini, Ann M.
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4561 - 4570
反应条件
(i) (diazotization), (ii) CuCl, KI, (iii) /BRN= 4161425/; Multistep reaction;
参考文献
Tulp Th.; Hutzinger
Biomedical Mass Spectrometry, 1978 , vol. 5, # 3 p. 224 - 231
