5-(叔丁基)-2-甲基苯并噁唑合成路线 （共 8 条）
反应条件
trichlorophosphate in 1,2-dichloro-ethane
T=93°C; Vilsmeier formylation; 3 h;
参考文献
Li, Ke-Lai; Du, Zong-Bo; Guo, Can-Cheng; Chen, Qing-Yun
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3286 - 3292
反应条件
in methanol
4 h; Heating / reflux;
参考文献
PHANOS TECHNOLOGIES, INC.
Patent: WO2007/61768 A2, 2007 ;
Location in patent: Page/Page column 20-21 ;
反应条件
trichlorophosphate in chloroform
T=73°C; Vilsmeier formylation; 3 h;
参考文献
Li, Ke-Lai; Du, Zong-Bo; Guo, Can-Cheng; Chen, Qing-Yun
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3286 - 3292
反应条件
1: tetrahydrofuran / 24 h / 20 °C / |Inert atmosphere; |Darkness
2: toluene-4-sulfonic acid / toluene / 90 °C / |Inert atmosphere
View Scheme
参考文献
Dulong, Florian; Thuery, Pierre; Ephritikhine, Michel; Cantat, Thibault
Organometallics, 2013 , vol. 32, # 5 p. 1328 - 1340
反应条件
in dichloromethane
T=60°C; 48 h; Inert atmosphere;
参考文献
Dulong, Florian; Thuery, Pierre; Ephritikhine, Michel; Cantat, Thibault
Organometallics, 2013 , vol. 32, # 5 p. 1328 - 1340
反应条件
1: sodium dithionite; aq. NaOH solution
2: acetic acid
View Scheme
参考文献
Anish
Patent: US2429178 , 1944 ;
参考文献
Anish
Patent: US2429178 , 1944 ;
Full Text Show Details
Gen. Aniline and Film Corp.
Patent: US2441342 , 1944 ;
参考文献
Anish
Patent: US2429178 , 1944 ;
Full Text Show Details
Gen. Aniline and Film Corp.
Patent: US2441342 , 1944 ;
