4-乙酰胺基-2,2,6,6-四甲基哌啶合成路线 （共 8 条）
反应条件
sodium hydroxide; acetic anhydride in water; isopropyl alcohol; toluene
参考文献
Ciba-Geigy Corporation
Patent: US5286865 A1, 1994 ;
反应条件
in diethyl ether T=5 - 10°C; 3.5 h;
参考文献
Zakrzewski, Jerzy; Krawczyk, Maria
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 1 p. 514 - 516
反应条件
sodium carbonate in water T=20°C; 1 h;
参考文献
Tilley, Leon J.; Bobbitt, James M.; Murray, Stephanie A.; Camire, Casey E.; Eddy, Nicholas A.
Synthesis (Germany), 2013 , vol. 45, # 3 art. no. SS-2012-M0631-PSP, p. 326 - 329
反应条件
sodium nitrite in water
参考文献
Kashparova; Kagan; Kashparov; Zhukova
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 4 p. 667 - 668
反应条件
1: N-(2,2,6,6-tetramethylpiperidin-4-yl)acetamide With dihydrogen peroxide; tungstate anion T=20°C; 144 h; 2: With water; potassium hydroxide 30 h; Reflux; 3: thiophosgene With triethylamine in benzene T=10 - 17°C;
参考文献
Zakrzewski, Jerzy; Krawczyk, Maria
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 1 p. 514 - 516
反应条件
1: H2O2 2: KOH 3: 65 percent / 5 percent NaOH / 0.17 h View Scheme
参考文献
Plessas; Goldstein
Carbohydrate research, 1981 , vol. 89, # 2 p. 211 - 220
参考文献
Tilley, Leon J.; Bobbitt, James M.; Murray, Stephanie A.; Camire, Casey E.; Eddy, Nicholas A.
Synthesis (Germany), 2013 , vol. 45, # 3 art. no. SS-2012-M0631-PSP, p. 326 - 329
反应条件
1: H2O2 2: KOH View Scheme
参考文献
Plessas; Goldstein
Carbohydrate research, 1981 , vol. 89, # 2 p. 211 - 220
