2-(甲氨基)-5-硝基吡啶合成路线 （共 32 条）
反应条件
1: 95 percent / PCl3 / CHCl3 / 1 h / Heating 2: 92 percent / 100percent N2H4 / ethanol / Heating 3: 28 percent / CH3COOAg / 1 h / Heating View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
1: 90 percent / 5 h / 120 °C 2: 73 percent / conc. H2SO4, HNO3(D=1.4) / 1 h / 60 °C 3: 83 percent / PCl3 / CHCl3 View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
1: 73 percent / conc. H2SO4, HNO3(D=1.4) / 1 h / 60 °C 2: 83 percent / PCl3 / CHCl3 View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
1: 92 percent / 100percent N2H4 / ethanol / Heating 2: 28 percent / CH3COOAg / 1 h / Heating View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
1: 51 percent / 100percent N2H4 / ethanol / 1.) 1 h, room temperature; 2.) 12 h, 0 deg C 2: 65 percent / CH3COOAg / H2O / 1 h / Heating 3: 83 percent / PCl3 / CHCl3 View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
1: 65 percent / CH3COOAg / H2O / 1 h / Heating 2: 83 percent / PCl3 / CHCl3 View Scheme
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
silver(I) acetate 1 h; Heating;
参考文献
Talik, Tadeusz; Talic, Zofia
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 1 p. 84 - 88
反应条件
4 h; Refluxneat (no solvent);
参考文献
Kodimuthali, Arumugam; Mungara, Anitha; Prasunamba, Padala Lakshmi; Pal, Manojit
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 8 p. 1439 - 1445
反应条件
29 h; Refluxneat (no solvent);
参考文献
Kodimuthali, Arumugam; Mungara, Anitha; Prasunamba, Padala Lakshmi; Pal, Manojit
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 8 p. 1439 - 1445
反应条件
sodium hydroxide in water T=60°C; Rate constant;
参考文献
Kijima, Atsushi; Sekiguchi, Shizen
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3597 - 3602
