1-[[(4-甲基苯基)磺酰基]氨基]-吡啶鎓氢氧化物内盐合成路线 （共 10 条）
反应条件
5A molecular sieve; copper(II) bis(trifluoromethanesulfonate) in acetonitrile
T=20°C; 8 h;
参考文献
Jain, Suman L.; Sharma, Vishal B.; Sain, Bir
Tetrahedron Letters, 2003 , vol. 44, # 23 p. 4385 - 4387
反应条件
4 A molecular sieve; [meso-tetrakis(p-tolyl)porphyrinato]ruthenium(II) in dichloromethane
T=30°C;
参考文献
Jiang, Yan; Zhou, Guo-Chuan; He, Guang-Li; He, Ling; Li, Ju-An; Zheng, Shi-Long
Synthesis, 2007 , # 10 p. 1459 - 1464
反应条件
triethylamine in tetrahydrofuran
T=70°C; Cooling with ice;
参考文献
Li, Chaoqun; Zhang, Liming
Organic Letters, 2011 , vol. 13, # 7 p. 1738 - 1741
反应条件
1: pyridine With O-(2,4-dinitro-phenyl)-hydroxylamine in tetrahydrofuran; water
T=40°C; 12 h;
2: p-toluenesulfonyl chloride With sodium hydroxide in tetrahydrofuran; water
T=20°C; 4 h;
参考文献
Zhao, Jingjing; Li, Pan; Wu, Chunrui; Chen, Hongli; Ai, Wenying; Sun, Renhong; Ren, Hailong; Larock, Richard C.; Shi, Feng
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 9 p. 1922 - 1930
反应条件
molecular sieve; tris(3,4,5-tribromopyrazol-1-yl)Cu(NCMe)
T=80°C;
参考文献
Fructos, Manuel R.; Trofimenko, Swiatoslaw; Mar Diaz-Requejo; Perez, Pedro J.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11784 - 11791
反应条件
sodium hydroxide in tetrahydrofuran; water
参考文献
Chong, Pek; Davis, Roman; Tabet, Elie; Elitzin, Vassil; Hatcher, Mark; Liu, Bing; Salmons, Matthew
Tetrahedron Letters, 2012 , vol. 53, # 50 p. 6786 - 6788,3
反应条件
T=160°C; P=55480 Torr; 1.5 h;
参考文献
Ayyangar, N. R.; Bambal, R. B.; Srinivasan, K. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 36 - 40
参考文献
Chang, Young Hwan; Chiu, Fang-Ting; Zon, Gerald
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 342 - 354
参考文献
Datta
Journal of the Indian Chemical Society, 1947 , vol. 24, p. 109,112
Full Text Show Details
Curtius; Vorbach
Journal fuer Praktische Chemie (Leipzig), 1930 , vol. <2>125, p. 340,343
反应条件
potassium acetate; copper diacetate in 1,4-dioxane
T=120°C; 16 h; Sealed tube;
参考文献
Ling, Lin; Chen, Jingqing; Song, Jiahui; Zhang, Yuhai; Li, Xinqian; Song, Lijuan; Shi, Feng; Li, Yuxue; Wu, Chunrui
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3894 - 3902
