N-亚硫酰基-p-甲苯磺胺合成路线 （共 35 条）
反应条件
thionyl chloride in tetrahydrofuran; benzene 10 h; Heating;
参考文献
Smyth, Timothy P.; O'Donnell, Michael E.; O'Connor, Michael J.; St Ledger, James O.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7600 - 7618
反应条件
in dichloromethane 1.) -40 deg C, 2.) 25 deg C, 1 h;
参考文献
Kim, Yong Hae; Shin, Jai Moo
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3821 - 3824
反应条件
1: CH2Cl2 / Ambient temperature 2: 80 percent / SOCl2 / 8 h / Heating View Scheme
参考文献
Smyth, Timothy P.; O'Donnell, Michael E.; O'Connor, Michael J.; St Ledger, James O.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7600 - 7618
反应条件
1: 35 mg / methanol / 0.03 h / Ambient temperature 2: CDCl3 / 6 h / 25 °C 3: 80 percent / SOCl2 / 8 h / Heating View Scheme
参考文献
Smyth, Timothy P.; O'Donnell, Michael E.; O'Connor, Michael J.; St Ledger, James O.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7600 - 7618
反应条件
in acetonitrile 1) -30 deg C; 2) 20 deg C, 20 min;
参考文献
Schwoebel, Alfred; Kresze, Guenter
Liebigs Annalen der Chemie, 1985 , # 3 p. 453 - 461
反应条件
triethylsilane; boron trifluoride diethyl etherate in benzene T=5°C;
参考文献
Alexander, Michael D.; Anderson, Robert E.; Sisko, Joseph; Weinreb, Steven M.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2563 - 2564
参考文献
Cram,D.J. et al.
Journal of the American Chemical Society, 1970 , vol. 92, # 25 p. 7369 - 7384
反应条件
1: 90 percent / toluene / 25 °C 2: 64 percent / Et3N, P(OCH3)3 / methanol / 25 °C View Scheme
参考文献
Harrington; Sanchez
Synthetic Communications, 1994 , vol. 24, # 2 p. 175 - 180
反应条件
tert-butyl alcohol in toluene T=90°C; 6 h;
参考文献
McFarland, John W.; Schut, Dirk; Zwanenburg, Binne
Tetrahedron, 1981 , vol. 37, p. 389 - 393
反应条件
in 1,2-dichloro-ethane T=0°C; 4 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 11 p. 3377 - 3378
