反应条件
in hexane; cyclohexane 1-bromooctane (1 equiv.) and TMTH (2 equiv.) in hexane cooled to 0°C under Ar, LDA (1 equiv., 1.6 M soln. in cyclohexane) dropped in, stirred for 20-25 min at room temp., quenched with water; analyzed by GC (after quenching), NMR (before quenching);
参考文献
Organometallics, , vol. 6, p. 557 - 565
