反应条件
in ethyl acetate
(Ar); soln. of Br2 in EtOAc was slowly added to stirred soln. of Et4Pb in EtOAc at -80°C until color of mixt. remained yellow; cold mixt. decanted; residue extd. (Et2O, room temp.); evapd.; dried (vac.);
参考文献
Mueller, Thomas; Bauch, Christian; Ostermeier, Markus; Bolte, Michael; Auner, Norbert
Journal of the American Chemical Society, 2003 , vol. 125, # 8 p. 2158 - 2168
