1,1,2,2-四甲基环丙烷合成路线 (共 33 条)
反应条件
tetrafluoroboric acid in dichloromethane T=-78°C;
参考文献
Casey,C.P.; Miles,W.H.; Tukada,H.
Journal of the American Chemical Society, 1985 , vol. 107, p. 2924
反应条件
diiodomethane; coppered zinc; iodine Reagens 4: Aether;
参考文献
Schlosser,M.; Heinz,G.
Angewandte Chemie, 1967 , vol. 79, # 13 p. 617 - 618
反应条件
hydrogen bromide Behandlung des in Aethanol geloesten Reaktionsprodukts mit Zinkstaub, anfangs in der Kaelte, zuletzt auf dem Dampfbad;
参考文献
Kelso et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1751,1754
反应条件
BF3·2HOAc in dichloromethane-d2 T=0°C; 0.25 h;
参考文献
Fleming, Ian; Urch, Christopher J.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 173 - 192
参考文献
Kelso et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1751,1754
反应条件
T=170°C; 12 h; Yield given. Yields of byproduct given;
参考文献
Kawa, Hajimu; Manley, Bobby C.; Lagow, Richard J.
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5313 - 5314
反应条件
copper; zinc in diethyl ether
参考文献
Kropp, Paul J.; Pienta, Norbert J.; Sawyer, Joy A.; Polniaszek, Richard P.
Tetrahedron, 1981 , vol. 37, # 19 p. 3229 - 3236
反应条件
(i) Et2O, (ii) H2O; Multistep reaction;
参考文献
Rudasheskaya, T. Yu.; Nesmeyanova, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 8 p. 1647 - 1650
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 8 p. 1821 - 1824
反应条件
lithium tert-butylate in tetrahydrofuran; tert-butyl alcohol
参考文献
Schlosser,M.; Heinz,G.
Angewandte Chemie, 1967 , vol. 79, # 13 p. 617 - 618
参考文献
Likhotvorik, Igor R.; Tippmann, Eric; Platz, Matthew S.
Tetrahedron Letters, 2001 , vol. 42, # 17 p. 3049 - 3051