1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=25°C; 1.5 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Prokofjevs, Aleksandrs; Boussonniere, Anne; Li, Linfeng; Bonin, Helene; Lacote, Emmanuel; Curran, Dennis P.; Vedejs, Edwin
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12281 - 12288
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=50°C; 2 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Prokofjevs, Aleksandrs; Boussonniere, Anne; Li, Linfeng; Bonin, Helene; Lacote, Emmanuel; Curran, Dennis P.; Vedejs, Edwin
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12281 - 12288
sodium peroxodisulphate; silver nitrate in water; acetonitrile Heating;
参考文献
Arnoldi, Claudio; Citterio, Attilio; Minisci, Francesco
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 531 - 542
Titanium substituted ZSM-5; dihydrogen peroxide in butanone T=80°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yiu, Shek-Man; Wu, Zhi-Biao; Mak, Chi-Keung; Lau, Tai-Chu
Journal of the American Chemical Society, 2004 , vol. 126, # 45 p. 14921 - 14929
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=50°C; 2 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Prokofjevs, Aleksandrs; Boussonniere, Anne; Li, Linfeng; Bonin, Helene; Lacote, Emmanuel; Curran, Dennis P.; Vedejs, Edwin
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12281 - 12288
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=25°C; 1.5 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Prokofjevs, Aleksandrs; Boussonniere, Anne; Li, Linfeng; Bonin, Helene; Lacote, Emmanuel; Curran, Dennis P.; Vedejs, Edwin
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12281 - 12288
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=25°C; 1.5 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=25°C; 16 h;
参考文献
Prokofjevs, Aleksandrs; Boussonniere, Anne; Li, Linfeng; Bonin, Helene; Lacote, Emmanuel; Curran, Dennis P.; Vedejs, Edwin
Journal of the American Chemical Society, 2012 , vol. 134, # 29 p. 12281 - 12288