2,6-二叔丁基-4-乙基苯酚合成路线 (共 22 条)
反应条件
in N,N-dimethyl-formamide 0.616667 h; electrolysis, n-Bu4NClO4;
参考文献
Phillips, J. Paige; Gillmore, Jason G.; Schwartz, Phillip; Brammer Jr., Larry E.; Berger, Daniel J.; Tanko
Journal of the American Chemical Society, 1998 , vol. 120, # 1 p. 195 - 202
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; chlorobenzene 1 h; Heating;
参考文献
Baik, Woonphil; Lee, Hyun Joo; Koo, Sangho; Kim, Byeong Hyo
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8125 - 8128
反应条件
potassium hydroxide; Pd/C; zinc(II) oxide T=200°C; 15 h;
参考文献
Krysin; Pokrovskii
Russian Journal of General Chemistry, 2008 , vol. 78, # 9 p. 1728 - 1733
参考文献
Stevens
Industrial and Engineering Chemistry, 1943 , vol. 35, p. 655,656
反应条件
sodium hydroxide; sodium tetrahydroborate in methanol T=30°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Nishinaga, Akira; Kojima, Shinya; Mashino, Takahiro; Maruyama, Kazushige
Chemistry Letters, 1994 , # 5 p. 961 - 964
反应条件
potassium hydroxide in ethanol T=230°C; 0.333333 h;
参考文献
Krysin; Pokrovskii
Russian Journal of General Chemistry, 2008 , vol. 78, # 9 p. 1728 - 1733
反应条件
aluminum oxide P=5 Torr; Heating; Yield given. Yields of byproduct given;
参考文献
Kamogawa, Hiroyoshi; Watanabe, Motoshi; Oka, Saichiro; Nanasawa, Masato
Chemistry Letters, 1980 , p. 793 - 794
反应条件
potassium hydroxide in ethanol T=230°C; 0.5 h;
参考文献
Krysin; Pokrovskii
Russian Journal of General Chemistry, 2008 , vol. 78, # 9 p. 1728 - 1733
反应条件
sodium hydroxide; ethanol T=225°C;
参考文献
Shell Devel. Co.
Patent: US2841623 , 1957 ;
反应条件
(i) KOtBu, tBuOH, (ii) NaH, PE; Multistep reaction. Further byproducts given;
参考文献
Kornblum,N.; Seltzer,R.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3668 - 3671