N-氯甲基苯并噻唑-2-硫酮合成路线 (共 9 条)
反应条件
triethylamine in benzene 4 h; Heating;
参考文献
Abdel-Rahman, M. A.; Ghattas, A.-B. A. G.; El-Saraf, G. A.; Khodary, A.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 85, # 1-4 p. 183 - 192
反应条件
acetic acid; zinc in benzene
参考文献
Stavrovskaya,V.I.; Kolosova,M.O.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 689 - 694,711 - 715
参考文献
Stawrowskaja; Kolosowa
Zhurnal Obshchei Khimii, 1960 , vol. 30, p. 689,691; engl. Ausg. S. 711, 712
反应条件
in acetone 24 h; Heating; Product distributionMechanism;
参考文献
D'Amico, John J.; Suba, Lydia; Ruminski, Peter G.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1479 - 1482
反应条件
thionyl chloride in water; 1,2-dichloro-ethane
2 h; Heating;
参考文献
D'Amico, John J.; Suba, Lydia; Ruminski, Peter G.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1479 - 1482
反应条件
1: 80 percent / ethanol; H2O / 0.17 h / 70 - 75 °C
2: 70 percent / POCl3, pyridine / 0.5 h / 60 - 70 °C
View Scheme
参考文献
Muthusubramanian, Lakshmi; Mitra, Rajat B.; Sundara Rao; Raghavan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1996 , vol. 35, # 12 p. 1331 - 1334
参考文献
D'Amico, John J.; Bollinger, Frederic G.; Dahl, William E.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 35, p. 71 - 76
反应条件
1: 98 percent / dimethylformamide
2: 90 percent / 30percent H2SO4
3: 94 percent / BF3*O(C2H5)2 / 24 h / Heating
View Scheme
参考文献
D'Amico, John J.; Bollinger, Frederic G.; Dahl, William E.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 35, p. 71 - 76
反应条件
1: 98 percent / dimethylformamide
2: 90 percent / 30percent H2SO4
View Scheme
参考文献
D'Amico, John J.; Suba, Lydia; Ruminski, Peter G.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1479 - 1482