lithium aluminium tetrahydride; cerium(III) chloride in not given 0-25°C; according to Imamoto, T. et al., J. Am. Chem. Soc., 1985, 107, 5301; IR and (1)H-NMR spectroscopy;
参考文献
Imamoto, Tsuneo; Kusumoto, Tetsuo; Suzuki, Nobuyo; Sato, Kazuhiko
Journal of the American Chemical Society, 1985 , vol. 107, # 18 p. 5301 - 5303
Fuller, Anna-Marie; Mountford, Andrew J.; Scott, Matthew L.; Coles, Simon J.; Horton, Peter N.; Hughes, David L.; Hursthouse, Michael B.; Lancaster, Simon J.
Inorganic Chemistry, 2009 , vol. 48, # 23 p. 11474 - 11482
in tetrahydrofuran under N2, Schlenk techniques; soln. of P compd. (13.5 mmol) added to soln. of B compd. (13.5 mmol) at -78°C with stirring, warmed to roomtemp. overnight; evapd., chromd. (SiO2, hexane:toluene=1:1), evapd., triturated (pentane), crystd.;
参考文献
Dornhaus, Franz; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
European Journal of Inorganic Chemistry, 2006 , # 9 p. 1777 - 1785
