1-(羟基-苯基-甲基)环戊烷-1-醇合成路线 （共 6 条）
反应条件
hydrogen; sodium hydride in toluene
T=20°C; P=750.075 Torr; 16 h;
参考文献
Schmidt, Bernd; Pohler, Michael
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 14 p. 2512 - 2517
反应条件
1: 89 percent / diethyl ether / 0 °C
2: 89 percent / cyclo-[(Mes)NCH2CH2N(Mes)CH]-RuCl2(PCy3)=CHPh / CH2Cl2 / 20 °C
3: 0.29 g / NaH; H2 / toluene / 16 h / 20 °C / 750.08 Torr
View Scheme
参考文献
Schmidt, Bernd; Pohler, Michael
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 14 p. 2512 - 2517
反应条件
1: 89 percent / cyclo-[(Mes)NCH2CH2N(Mes)CH]-RuCl2(PCy3)=CHPh / CH2Cl2 / 20 °C
2: 0.29 g / NaH; H2 / toluene / 16 h / 20 °C / 750.08 Torr
View Scheme
参考文献
Schmidt, Bernd; Pohler, Michael
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 14 p. 2512 - 2517
反应条件
1: H2 / Raney-Ni
2: O2
View Scheme
参考文献
Chirko,A.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 26 - 30
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, # 1 p. 28 - 33
参考文献
Chirko,A.I. et al.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 26 - 30
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, # 1 p. 28 - 33
参考文献
Elphimoff-Felkin; Tchoubar
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1953 , vol. 237, p. 726
