5,6,7,8-四氢-1-萘甲醇合成路线 (共 14 条)
反应条件
1: diluted Cr2O3-H2SO4 2: permanganate View Scheme
参考文献
Wightman,R.H. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 11 p. 2167 - 2170
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
1: SOCl2; pyridine; toluene 2: ethanol / Erwaermen des Reaktionsprodukts mit wss. NaOH 3: palladium/charcoal View Scheme
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
thionyl chloride in toluene 2 h;
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
potassium hydrogensulfate; LiAlH4 in tetrahydrofuran; diethyl ether
参考文献
Warner-Lambert Company
Patent: US5610177 A1, 1997 ;
US 5610177 A
反应条件
sodium tetrahydroborate in ethanol
1.5 h;
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
1: 75 percent / H2 / Pd/C / acetic acid / 6 h
2: 87 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
View Scheme
参考文献
Connolly, Terrence J.; Durst, Tony
Tetrahedron, 1997 , vol. 53, # 47 p. 15969 - 15982
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Newman; Bye
Journal of the American Chemical Society, 1952 , vol. 74, p. 905,907
反应条件
acetic acid; zinc; Co catalyst
参考文献
Fischli
Helvetica Chimica Acta, 1979 , vol. 62, # 3 p. 882 - 893
反应条件
acetic acid; zinc; Co catalyst
参考文献
Fischli
Helvetica Chimica Acta, 1979 , vol. 62, # 3 p. 882 - 893