4'-乙酰苯并-18-冠-6-醚合成路线 （共 10 条）
反应条件
PPA T=70°C; 0.666667 h;
参考文献
Shkinev, A. V.; Asrarov, M. I.; Gagel'gans, A. I.; Saifullina, N. Zh.; Mukhamedzhanova, E. A.; Tashmukhamedova, A. K.
Chemistry of Natural Compounds, 1983 , vol. 19, # 5 p. 597 - 600
Khimiya Prirodnykh Soedinenii, 1983 , # 5 p. 634 - 637
反应条件
PPA in acetic acid T=60°C;
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
chromium(VI) oxide; sulfuric acid in acetone Yield given;
参考文献
Arias; Echegoyen; Wilson; Lu
Journal of the American Chemical Society, 1995 , vol. 117, # 4 p. 1422 - 1427
反应条件
iron(III) oxide T=20°C; Friedel Crafts acylation; 0.5 h; regioselective reaction;
参考文献
Sharghi, Hashem; Jokar, Mahboubeh; Doroodmand, Mohammad Mahdi; Khalifeh, Reza
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 17 p. 3031 - 3044
反应条件
sodium carbonate in acetone T=50 - 60°C; 65 h; Yield given;
参考文献
Alonso, Maria Teresa; Brunet, Ernesto; Hernandez, Concepcion; Rodriguez-Ubis, Juan Carlos
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7465 - 7468
反应条件
sodium hydroxide in water; butan-1-ol 72 h; Heating;
参考文献
Fenton, David E.; Parkin, Donald; Newton, Roger F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 449 - 454
反应条件
2: 78 percent / polyphosphoric acid / acetic acid / 60 °C View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
2: 78 percent / polyphosphoric acid / acetic acid / 60 °C View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
反应条件
1: 1.) potassium hydroxide, 2.) sodium hydroxide / 1.) 140 deg C, 5 d, 2.) dioxane, water, 14 h 2: 48 percent / sodium hydroxide / H2O; butan-1-ol / 72 h / Heating View Scheme
参考文献
Fenton, David E.; Parkin, Donald; Newton, Roger F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 449 - 454
反应条件
1: 92 percent / sodium borohydride / ethanol / 18 h / Ambient temperature 2: 93 percent / pyridinium tosylate / benzene / 18 h / Heating View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
