2,4-二溴-6-溴甲基苯酚合成路线 （共 19 条）
反应条件
sulfuric acid; hydrogen bromide in acetic acid T=80°C;
参考文献
RAMOT AT TEL-AVIV UNIVERSITY LTD.; KOL, Moshe; PRESS, Konstantin; COHEN, Ad
Patent: WO2011/158241 A1, 2011 ;
Location in patent: Page/Page column 49 ;
反应条件
bromine in tetrachloromethane 8 h; Irradiation;
参考文献
Brittain, Judith M.; Mare, Peter B. D. de la; Newman, Paul A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 32 - 41
反应条件
hydrogen bromide in acetic acid T=70°C; 12 h;
参考文献
Wang, Yuan; Ma, Haiyan
Chemical Communications, 2012 , vol. 48, # 53 p. 6729 - 6731
参考文献
Brittain, Judith M.; Mare, Peter B. D. de la; Newman, Paul A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 32 - 41
反应条件
1: sodium tetrahydroborate / methanol / 3.5 h 2: sulfuric acid; hydrogen bromide / acetic acid / 80 °C View Scheme
参考文献
RAMOT AT TEL-AVIV UNIVERSITY LTD.; KOL, Moshe; PRESS, Konstantin; COHEN, Ad
Patent: WO2011/158241 A1, 2011 ;
参考文献
Zincke; Hedenstroem
Justus Liebigs Annalen der Chemie, 1906 , vol. 350, p. 275
反应条件
diethyl ether; chloroform; bromine man verreibt das Reaktionsprodukt mit Wasser;
参考文献
Auwers; Buettner
Justus Liebigs Annalen der Chemie, 1898 , vol. 302, p. 145
反应条件
Ambient temperature;
参考文献
Brittain, Judith M.; Mare, Peter B. D. de la; Newman, Paul A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 32 - 41
反应条件
man erhitzt dann auf 115-120grad und fuegt Brom hinzu;
参考文献
Auwers; Schroeter
Justus Liebigs Annalen der Chemie, 1906 , vol. 344, p. 160
参考文献
Auwers; Buettner
Justus Liebigs Annalen der Chemie, 1898 , vol. 302, p. 145
Full Text Show Details
Auwers
Chemische Berichte, 1901 , vol. 34, p. 4256
Chemische Berichte, 1906 , vol. 39, p. 3160
