2-甲酰基苯氧基醋酸乙酯合成路线 (共 16 条)
反应条件
potassium carbonate in acetone T=20°C; 5 h;
参考文献
Bello, Angelica M.; Wei, Lianhu; Majchrzak-Kita, Beata; Salum, Norue; Purohit, Meena K.; Fish, Eleanor N.; Kotra, Lakshmi P.
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 978 - 985
反应条件
alum in neat (no solvent) T=80°C; 12 h; Green chemistry; TemperatureTime;
参考文献
Shunmugadhas, Ganesan; Kumar, Suresh; Kumaresan, Sudalaiandi
Journal of Chemical Sciences (Bangalore), 2012 , vol. 124, # 4 p. 857 - 863,7
反应条件
potassium carbonate in acetone 20 h; Heating;
参考文献
Kattner; Gohring; Hartmann
Archiv der Pharmazie, 1995 , vol. 328, # 3 p. 239 - 245
反应条件
potassium carbonate in N,N-dimethyl-formamide T=92 - 96°C; Substitution; 2 h;
参考文献
Kwiecien
Polish Journal of Chemistry, 1998 , vol. 72, # 10 p. 2254 - 2260
参考文献
Sanofi
Patent: US5736548 A1, 1998 ;
反应条件
1: 2-methyl-benzyl alcohol With potassium hydroxide in methanol T=50°C; 0.5 h; 2: ethyl bromoacetate in methanol; N,N-dimethyl-formamide T=0 - 25°C;
参考文献
D'Sa, Bosco A.; Kisanga, Philip; Verkade, John G.
Synlett, 2001 , # 5 p. 670 - 672
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Syrbu, S. A.; Semeikin, A. S.; Berezin, B. D.; Koifman, O. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 10 p. 1149 - 1153
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , vol. 25, # 10 p. 1373 - 1377
反应条件
1: sodium hydroxide / water / 3 h / |Reflux 2: alum / 12 h / |Reflux; |Green chemistry View Scheme
参考文献
Suresh Kumar; Antony Muthu Prabhu; Seethalaksmi; Bhuvanesh; Kumaresan
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2014 , vol. 123, p. 249 - 256
反应条件
di-tert-butyl peroxide in various solvent(s) T=150°C; 14 h;
参考文献
Woergoetter, Erich; Hohenlohe-Oehringen, Kraft
Monatshefte fuer Chemie, 1985 , vol. 116, p. 995 - 1004
反应条件
alum 12 h; RefluxGreen chemistry;
参考文献
Suresh Kumar; Kumaresan; Antony Muthu Prabhu; Bhuvanesh; Seethalakshmi
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 101, p. 254 - 263