反应条件
1: 88 percent / K3<Fe(CN)6>, K2CO3, bis(9-O-dihydroquinidinyl)terephthalate, OsO4 / 2-methyl-propan-2-ol; H2O; toluene / 0.83 h / 25 °C 2: 100 percent / SOCl2, Et3N / CH2Cl2 / 3 h 3: NaN3 / dimethylformamide / 6 h / 50 °C 4: 96 percent / Et3N / CH2Cl2 / 0 °C 5: H2 / Pd/C 6: 1.) diethyl azodicarboxylate, PPh3, 2.) 1N aq. NaOH / 2.) MeOH, 2 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 6 p. 471 - 473
