in neat (no solvent) SF4 added by vac. distillation to cooled (CH3)3SiNHTeF5 and mixt. allowed to react. at room temp. overnight with stirring; contens separated by slow vac. distillation through -20 (H2NTeF5), -65 (F2S=NTeF5) and -196°C ((CH3)3SiF and SF4) traps; elem. anal.;
参考文献
Hartl, Hans; Huppmann, Peter; Lentz, Dieter; Seppelt, Konrad
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Krolevets, A. A.; Popov, A. G.; Adamov, A. V.; Martynov, I. V.
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