反应条件
in neat (no solvent)
adding PI2(CF3) to H2O in vacuum at 20°C, after 2 h further H2O and H2O2 (dropwise) are added, I2 is filtered off and soln. is concentrated in 6 days in the cold;; heating light brown, moisture sensitive residue at 0.003 Torr to 85°C;;
参考文献
Bennett, F. W.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1954 , p. 3598 - 3603
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Gmelin Handbook: P: MVol.C, 273, page 626 - 629
