4,4-二甲氧基丁酸甲酯合成路线 （共 24 条）
反应条件
sulfuric acid in methanol Substitution;
参考文献
Yu, Peng; Wang, Tao; Li, Jin; Cook, James M.
Journal of Organic Chemistry, 2000 , vol. 65, # 10 p. 3173 - 3191
反应条件
sulfuric acid in methanol 3 h; Ambient temperature;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3338 - 3340
反应条件
1: 4-nitrobutyric acid methyl ester With sodium methylate in methanol 2: methanol With sulfuric acid
参考文献
Davies, Stephen G.; Roberts, Paul M.; Stephenson, Peter T.; Storr, Helen R.; Thomson, James E.
Tetrahedron, 2009 , vol. 65, # 39 p. 8283 - 8296
反应条件
tetrabutylammonium fluoride; triethylamine T=18 - 20°C; electrolysis: constant current = 2.5 A (current density = 62.5 mA/cm2), initial voltage = 14 V, final voltage = 40 V, amount of electricity passed = 8 F/mol;
参考文献
Iwasaki, Tameo; Nishitani, Takashi; Horikawa, Hiroshi; Inoue, Ichizo
Journal of Organic Chemistry, 1982 , vol. 47, # 19 p. 3799 - 3802
反应条件
carbonylchlorohydridetris(triphenylphosphine) ruthenium(II) T=150°C; 12 h;
参考文献
Hirai, Kenji; Suzuki, Hiroharu; Kashiwagi, Hiroshi; Moro-Oka, Yoshihiko; Ikawa, Tsuneo
Chemistry Letters, 1982 , p. 23 - 26
反应条件
lithium chloride in N,N-dimethyl-formamide Heating;
参考文献
Bernard, Angela M.; Piras, Pier Paolo; Toriggia, Paola
Synthesis, 1990 , # 6 p. 527 - 529
反应条件
1: 65 percent / tetraethylammonium p-toluenesulfonate / electrolysis (3 F/mol, 0.5 A) 2: 89 percent / 5percent H2SO4 / methanol / 3 h / Ambient temperature View Scheme
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1983 , vol. 48, # 19 p. 3338 - 3340
反应条件
triethylamine T=120°C; 192 h;
参考文献
Mialhe,Y.; Vessiere,R.
Bulletin de la Societe Chimique de France, 1970 , p. 3651 - 3656
反应条件
triethylamine T=120°C; 624 h;
参考文献
Mialhe,Y.; Vessiere,R.
Bulletin de la Societe Chimique de France, 1970 , p. 3651 - 3656
反应条件
sulfuric acid T=116°C;
参考文献
Ducher
Bulletin de la Societe Chimique de France, 1959 , p. 1259,1263
