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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4249-72-3
合成路线
（共 27 条）
4249-72-3
→
反应条件
40515-89-7
苯氧基乙苯
反应条件
formic acid; 5 palladium on charcoal in ethanol; water T=80°C; 1 h;
参考文献
Galkin, Maxim V.; Sawadjoon, Supaporn; Rohde, Volker; Dawange, Monali; Samec, Joseph S. M.
ChemCatChem, 2014 , vol. 6, # 1 p. 179 - 184
4249-72-3
→
反应条件
98-85-1
DL-1-苯乙醇
+
108-95-2
苯酚
反应条件
lithium aluminium tetrahydride; iron (III) acetylacetonate; sodium t-butanolate in toluene T=140°C; 24 h; Inert atmosphere; Temperature;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 48 p. 12674 - 12678
Angew. Chem., , vol. 125, # 48 p. 12906 - 12910
617-86-7
三乙基硅烷
+
4249-72-3
→
反应条件
5888-66-4
+
14629-62-0
反应条件
tris(pentafluorophenyl)-borane in dichloromethane T=20°C; 2 h; Inert atmosphere; Overall yield = 94 percent;
参考文献
Feghali, Elias; Cantat, Thibault
Chemical Communications, 2014 , vol. 50, # 7 p. 862 - 865
4249-72-3
+
100-51-6
苯甲醇
→
反应条件
1083-30-3
ω-苄基苯乙酮
反应条件
1: 2-phenoxy-1-phenylethanol With tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene T=140°C; 8 h; Schlenk techniqueSealed tubeInert atmosphere; 2: benzyl alcohol With potassium hydroxide in toluene T=140°C; 16 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Weickmann, Daniel; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 8 p. 2170 - 2173
4249-72-3
→
反应条件
1193-81-3
1-环己基乙醇
+
108-93-0
环己醇
反应条件
isopropyl alcohol T=100°C; 24 h; Concentration; Overall yield = 90 percentSpectr.;
参考文献
KAT2BIZ AB; SAMEC, Joseph; GALKIN, Maxim
Patent: WO2014/38989 A1, 2014 ;
Location in patent: Page/Page column 6 ;
4249-72-3
→
反应条件
60-12-8
苯乙醇
反应条件
copper oxides/alumina; hydrogen in ethyl acetate T=150°C; P=18751.9 Torr; 21 h; Inert atmosphereAutoclave;
参考文献
Strassberger, Zea; Alberts, Albert H.; Louwerse, Manuel J.; Tanase, Stefania; Rothenberg, Gadi
Green Chemistry, 2013 , vol. 15, # 3 p. 768 - 774
4249-72-3
→
反应条件
98-85-1
DL-1-苯乙醇
+
108-95-2
苯酚
反应条件
lithium aluminium tetrahydride; iron (III) acetylacetonate; sodium t-butanolate in toluene T=140°C; 24 h; Inert atmosphere; Temperature;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 48 p. 12674 - 12678
Angew. Chem., , vol. 125, # 48 p. 12906 - 12910
98-00-0
糠醇
+
4249-72-3
→
反应条件
2207-63-8
反应条件
1: 2-phenoxy-1-phenylethanol With tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene T=140°C; 8 h; Schlenk techniqueSealed tubeInert atmosphere; 2: 2-(hydroxymethyl)furan With potassium hydroxide in toluene T=140°C; 16 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Weickmann, Daniel; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 8 p. 2170 - 2173
4249-72-3
+
100-49-2
环己基甲醇
→
反应条件
28861-24-7
反应条件
1: 2-phenoxy-1-phenylethanol With tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene T=140°C; 8 h; Schlenk techniqueSealed tubeInert atmosphere; 2: cyclohexylmethyl alcohol With potassium hydroxide in toluene T=140°C; 16 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Weickmann, Daniel; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 8 p. 2170 - 2173
4249-72-3
→
反应条件
64-18-6
甲酸
+
721-04-0
2’-苯氧基苯乙酮
+
65-85-0
苯甲酸
+
108-95-2
苯酚
反应条件
(dipic)V(O)OiPr in dimethylsulfoxide-d6 T=100°C; 168 h; Under air;
参考文献
Hanson, Susan K.; Baker, R. Tom; Gordon, John C.; Scott, Brian L.; Thorn, David L.
Inorganic Chemistry, 2010 , vol. 49, # 12 p. 5611 - 5618
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