N-叔丁基-4-氯苯甲酰胺合成路线 （共 12 条）
反应条件
thionyl chloride Ambient temperature;
参考文献
Cawkill, Eric; Clark, Nigel G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 244 - 248
反应条件
in dichloromethane
T=0 - 25°C; 1.75 h; Inert atmosphere;
参考文献
Crestey, Francois; Knochel, Paul
Synthesis, 2010 , # 7 art. no. T22409SS, p. 1097 - 1106
反应条件
Amberlyst-15
T=70°C; Ritter type reaction; 2 h;
参考文献
Mokhtary, Masoud; Najafizadeh, Faranak
E-Journal of Chemistry, 2012 , vol. 9, # 2 p. 576 - 582
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
water; caesium carbonate in acetone
T=0°C; 0.333333 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: US6384033 B1, 2002 ;
反应条件
acetic acid; sodium nitrite in water; acetonitrile
T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Basavanag, Unnamatla M. V.; Dos Santos, Aurelie; El Kaim, Laurent; Gamez-Montano, Rocio; Grimaud, Laurence
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7194 - 7197
Angew. Chem., 2013 , vol. 125, # 28 p. 7335 - 7338,4
反应条件
oxygen; isovaleraldehyde in dichloromethane
T=0°C; 3 h;
参考文献
Martiny, Lars; Joergensen, Karl Anker
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 6 p. 699 - 704
反应条件
1: hydrofluoroboric acid; sodium nitrite / water / 0.58 h / 0 °C
2: caesium carbonate; water / acetone / 0.33 h / 0 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
potassium permanganate in water; acetonitrile
T=50°C; 0.5 h;
参考文献
Larsen, Jan; Jorgensen, Karl Anker; Christensen, Dorthe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1187 - 1190
