反式-1,2-环辛烷二醇合成路线 （共 15 条）
反应条件
(4-methoxyphenyl)-boronic acid; potassium carbonate; dibromoisocyanuric acid in water T=0°C; 4 h; DarknessElectrochemical reactionGreen chemistry; Reagent/catalyst;
参考文献
William, Julius M.; Kuriyama, Masami; Onomura, Osamu
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 934 - 940
反应条件
dimethyl sulfoxide; molybdenum peroxide in toluene Heating;
参考文献
Masuyama, Yoshiro; Usukura, Masa-aki; Kurusu, Yasuhiko
Chemistry Letters, 1982 , p. 1951 - 1952
反应条件
molybdenum peroxide in toluene Heating;
参考文献
Masuyama, Yoshiro; Usukura, Masa-aki; Kurusu, Yasuhiko
Chemistry Letters, 1982 , p. 1951 - 1952
反应条件
oxygen; potassium carbonate; Ru(PPh3)3Cl2/CW in various solvent(s) T=60°C; P=760.051 Torr; 15 h;
参考文献
Takezawa, Eiichiro; Sakaguchi, Satoshi; Ishii, Yasutaka
Organic Letters, 1999 , vol. 1, # 5 p. 713 - 715
反应条件
potassium carbonate 2.7 h; Ambient temperatureelectrolysis: nickel(III) oxide hydroxide electrode, 0.3 A;
参考文献
Ruholl, Heinrich; Schaefer, Hans J.
Synthesis, 1988 , # 1 p. 54 - 56
反应条件
dihydrogen peroxide; PCWP in 1,2-dichloro-ethane 12 h; Heating;
参考文献
Iwahama, Takahiro; Sakaguchi, Satoshi; Nishiyama, Yutaka; Ishii, Yasutaka
Tetrahedron Letters, 1995 , vol. 36, # 9 p. 1523 - 1526
反应条件
Boc-L-(π-Me)-His-(A)Gly-L-Cha-L-Phe-OMe in toluene
T=0°C; 5 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Mueller, Christian E.; Wanka, Lukas; Jewell, Kevin; Schreiner, Peter R.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 33 p. 6180 - 6183
反应条件
Boc-L-(π-Me)-His-(A)Gly-L-Cha-L-Phe-OMe; diisopropyl-carbodiimide in toluene
T=0°C; Steglich esterification; 18 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Hrdina, Radim; Mueller, Christian E.; Schreiner, Peter R.
Chemical Communications, 2010 , vol. 46, # 15 p. 2689 - 2690
反应条件
2,3-butanediol dehydrogenase from Bacillus subtilis in aq. buffer
T=30°C; pH=8; 6 h; Enzymatic reaction; Reagent/catalyst; enantioselective reaction;
参考文献
Zhang, Jiandong; Xu, Tingting; Li, Zhi
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3147 - 3153
反应条件
1: (+/-)-trans-1,2-cyclooctanediol With (5aS,10bR)-9-nitro-2-phenyl-4,5a,6,10b-tetrahydroindeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazin-2-ium tetrafluoroborate; 4-(N,N-dimethylamino)benzoic acid; N,N,N',N'-tetra-methylnaphthalene-1,8-diamine in chloroform
T=20°C; 0.166667 h;
2: 2-bromo-3-phenylpropanal in chloroform
T=0°C; 8 h;
参考文献
Kuwano, Satoru; Harada, Shingo; Kang, Bubwoong; Oriez, Raphael; Yamaoka, Yousuke; Takasu, Kiyosei; Yamada, Ken-Ichi
Journal of the American Chemical Society, 2013 , vol. 135, # 31 p. 11485 - 11488
