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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5-乙基四氢化萘
合成路线
（共 25 条）
92013-32-6
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
hydrogen; platinum(IV) oxide in tetrahydrofuran P=1034.3 Torr;
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
1127-76-0
1-乙基萘
→
反应条件
42775-75-7
5-乙基四氢化萘
+
13556-58-6
反应条件
copper oxide-chromium oxide T=195 - 225°C; P=77228.3 - 102971 Torr; Hydrogenation;
参考文献
Hipsher; Wise
Journal of the American Chemical Society, 1954 , vol. 76, p. 1747
52910-30-2
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
1: 2,6-lutidine / acetone; H2O 2: Pd-C / ethyl acetate View Scheme
参考文献
Thompson,G.L. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 3177 - 3190
52910-45-9
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
palladium on activated charcoal in ethyl acetate
参考文献
Thompson,G.L. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 3177 - 3190
119-64-2
1,2,3,4-四氢萘
+
60-29-7
乙醚
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
T=300°C; P=22065.2 Torr; Leiten ueber wenig Aluminiumoxyd enthaltendes Siliciumdioxyd;
参考文献
Kutz et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4026,4030
119-64-2
1,2,3,4-四氢萘
+
64-17-5
乙醇
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
T=300°C; P=22065.2 Torr; Leiten ueber wenig Aluminiumoxyd enthaltendes Siliciumdioxyd;
参考文献
Kutz et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4026,4030
119-64-2
1,2,3,4-四氢萘
+
54509-73-8
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
T=300°C; P=22065.2 Torr; Leiten ueber wenig Aluminiumoxyd enthaltendes Siliciumdioxyd;
参考文献
Kutz et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4026,4030
1074-15-3
邻溴苯乙基溴
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
1: 63 percent / NaOEt / 7 h / Heating 2: 98 percent / KOH / ethanol; H2O / 6 h / Heating 3: 95 percent / 170 °C 4: thionyl chloride / 0.75 h / Heating 5: 85 percent / AlCl3 / CS2 / 3 h / Heating 6: 89 percent / NaBH4 / ethanol; tetrahydrofuran 7: 96 percent / p-toluenesulfonic acid / benzene / Heating 8: 97 percent / NiCl2<dppp>2 / diethyl ether / Heating 9: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
19472-74-3
邻溴氰苄
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
1: 91 percent / sulfuric acid / H2O / 4 h / Heating 2: 84 percent / LiAlH4 / diethyl ether / 1 h / Heating 3: 72 percent / 48percent HBr, H2SO4 / 3 h / Heating 4: 63 percent / NaOEt / 7 h / Heating 5: 98 percent / KOH / ethanol; H2O / 6 h / Heating 6: 95 percent / 170 °C 7: thionyl chloride / 0.75 h / Heating 8: 85 percent / AlCl3 / CS2 / 3 h / Heating 9: 89 percent / NaBH4 / ethanol; tetrahydrofuran 10: 96 percent / p-toluenesulfonic acid / benzene / Heating 11: 97 percent / NiCl2<dppp>2 / diethyl ether / Heating 12: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
18698-97-0
邻溴苯乙酸
→
反应条件
42775-75-7
5-乙基四氢化萘
反应条件
1: 84 percent / LiAlH4 / diethyl ether / 1 h / Heating 2: 72 percent / 48percent HBr, H2SO4 / 3 h / Heating 3: 63 percent / NaOEt / 7 h / Heating 4: 98 percent / KOH / ethanol; H2O / 6 h / Heating 5: 95 percent / 170 °C 6: thionyl chloride / 0.75 h / Heating 7: 85 percent / AlCl3 / CS2 / 3 h / Heating 8: 89 percent / NaBH4 / ethanol; tetrahydrofuran 9: 96 percent / p-toluenesulfonic acid / benzene / Heating 10: 97 percent / NiCl2<dppp>2 / diethyl ether / Heating 11: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
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