1-(4-氯-苯基)-吡咯烷合成路线 (共 14 条)
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; triethylamine; bis[2-(diphenylphosphino)phenyl] ether in toluene
T=20°C; Inert atmosphereReflux;
参考文献
Hamid, M. Haniti S. A.; Allen, C. Liana; Lamb, Gareth W.; Maxwell, Aoife C.; Maytum, Hannah C.; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 1766 - 1774
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; TBPM in dimethyl sulfoxide
T=25°C; 24 h; Inert atmosphere;
参考文献
Yang, Chu-Ting; Fu, Yao; Huang, Yao-Bing; Yi, Jun; Guo, Qing-Xiang; Liu, Lei
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7398 - 7401
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7534 - 7537
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=25°C; 6 h; Inert atmosphere;
参考文献
Arundhathi, Racha; Kumar, Desitti Chaitanya; Sreedhar, Bojja
European Journal of Organic Chemistry, 2010 , # 19 p. 3621 - 3630
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol
T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
in 1-methyl-pyrrolidin-2-one
T=200 - 204°C; 0.75 h; microwave irradiation;
参考文献
Xu, Gang; Wang, Yan-Guang
Organic Letters, 2004 , vol. 6, # 6 p. 985 - 987
反应条件
potassium carbonate in water
T=100°C; 1 h; Microwave irradiation;
参考文献
Li, Hong Bo; Liang, Wu; Liu, Lang; Chen, Kai; Wu, Yi
Chinese Chemical Letters, 2011 , vol. 22, # 3 p. 276 - 279
反应条件
potassium hydroxide; pentacarbonyliron(0); carbon monoxide in ethanol; water
12 h; Ambient temperature;
参考文献
Shim, Sang Chul; Huh, Keun Tai; Park, Woo Hiun
Tetrahedron, 1986 , vol. 42, # 1 p. 259 - 264
反应条件
Shvo catalyst in 1,1-dimethylpropan-1-ol
T=150°C; 24 h;
参考文献
Hollmann, Dirk; Baehn, Sebastian; Tillack, Annegret; Parton, Rudy; Altink, Rinke; Beller, Matthias
Tetrahedron Letters, 2008 , vol. 49, # 40 p. 5742 - 5745
参考文献
Leoppky, Richard N.; Tomasik, Witold
Journal of Organic Chemistry, 1983 , vol. 48, # 16 p. 2751 - 2757
反应条件
N-ethyl-N,N-diisopropylamine in toluene
Heating;
参考文献
Cheng; Zhan; Meth-Cohn
Synthesis, 2002 , # 1 p. 34 - 38