呋喃-2,5-二甲酸二甲酯合成路线 （共 29 条）
反应条件
oxygen T=130°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
Journal of Catalysis, , vol. 265, # 1 p. 109 - 116
反应条件
1: furan-2-carboxylic acid With n-butyllithium in THF-d8 (tetrahydrofuran-d8); hexane T=-78°C; 0.333333 h; 2: methoxycarbonyl cyanide in tetrahydrofuran; hexane T=-78 - 20°C; 4 h; 3: diazomethane in diethyl ether T=-78°C; Overall yield = 44 percent; Overall yield = 81 mg;
参考文献
Journal of Natural Products, , vol. 75, # 10 p. 1765 - 1776
反应条件
1: furan-2-carboxylic acid With n-butyllithium in tetrahydrofuran T=-78°C; 2: carbon dioxide T=-78°C; 3: methanol With chloro-trimethyl-silane 2 h; Reflux;
参考文献
Arkivoc, , vol. 2013, # 4 p. 405 - 412
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C 1.2: -78 - 20 °C 2.1: toluene-4-sulfonic acid / water; toluene / 16 h / Reflux View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 32 p. 7346 - 7349
反应条件
1: hydrogenchloride / water / 4 h 2: copper(l) iodide; dihydrogen peroxide / 6 h / 140 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 62, # 1 p. 93 - 97
Izv. Akad. Nauk, Ser. Khim., , vol. 62, # 1 p. 93 - 97
反应条件
1.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran / 1.3 h / |Inert atmosphere; |Sealed tube 1.2: 0.5 h / -78 - 0 °C / |Inert atmosphere; |Sealed tube 1.3: 2 h / 80 °C / |Inert atmosphere; |Sealed tube 2.1: chloro-trimethyl-silane / methanol / 2 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Arkivoc, , vol. 2013, # 4 p. 405 - 412
参考文献
Polish Journal of Chemistry, , vol. 75, # 12 p. 1943 - 1946
反应条件
toluene-4-sulfonic acid in water; toluene 16 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 32 p. 7346 - 7349
反应条件
copper acetylacetonate T=150°C; 6 h; Inert atmosphereAutoclave;
参考文献
Russian Chemical Bulletin, , vol. 62, # 1 p. 93 - 97
Izv. Akad. Nauk, Ser. Khim., , vol. 62, # 1 p. 93 - 97
反应条件
copper acetylacetonate T=150°C; 6 h; Inert atmosphereAutoclave; Reagent/catalyst;
参考文献
Russian Chemical Bulletin, , vol. 62, # 1 p. 93 - 97
Izv. Akad. Nauk, Ser. Khim., , vol. 62, # 1 p. 93 - 97
