3-(4-硝基苯基)-吡啶合成路线 （共 39 条）
反应条件
potassium hydroxide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide in tetrahydrofuran
2 h; Heating;
参考文献
Ishikura, Minoru; Kamada, Machiko; Terashima, Masanao
Heterocycles, 1984 , vol. 22, # 2 p. 265 - 268
反应条件
1.1: n-butyllithium / diethyl ether / 2 h / -78 °C
1.2: 3 h / -78 °C
2.1: C52H67ClFeNPPd; copper(l) iodide; cesium fluoride / N,N-dimethyl-formamide / 12 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
in dimethyl sulfoxide
T=20°C; Arylation; 1 h;
参考文献
Gurczynski, Marek; Tomasik, Piotr
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 438 - 441
反应条件
acetic acid; acetyl chloride
参考文献
Forsyth; Pyman
Journal of the Chemical Society, 1926 , p. 2920
Journal of the Chemical Society, 1930 , p. 398
Full Text Show Details
Tschitschibabin; Schemjakina
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1921 , vol. 53, p. 217,223
Chem. Zentralbl., 1923 , vol. 94, # III p. 1024
参考文献
Ford; Mackay
Journal of the Chemical Society, 1958 , p. 1290,1294
反应条件
1: diethyl ether; H2O2; pyridine / -70 °C
2: nitrobenzene
View Scheme
参考文献
Ford; Mackay
Journal of the Chemical Society, 1958 , p. 1290,1294
参考文献
Elks; Hey
Journal of the Chemical Society, 1943 , p. 441,443
参考文献
Haworth et al.
Journal of the Chemical Society, 1940 , p. 349,352
反应条件
KO2
4 h; Ambient temperature; Further byproducts given;
参考文献
Crank, George; Gately, Garry E.; Makin, Mohammad I. H.
Australian Journal of Chemistry, 1984 , vol. 37, # 12 p. 2499 - 2507
反应条件
hydrogenchloride; sodium nitrite
2.) 40 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Byron; Lacey; Wilson
Molecular crystals and liquid crystals, 1980 , vol. 62, # 1-2 p. 103 - 114
