(4-氨基苯甲酰基)-1-哌啶合成路线 (共 7 条)
反应条件
hydrogen; palladium 10 on activated carbon in ethanol
参考文献
IRM LLC
Patent: US2005/124637 A1, 2005 ;
Location in patent: Page/Page column 9 ;
US 20050124637 A1
反应条件
dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate in 1,4-dioxane T=50°C; 24 h; Inert atmosphere;
参考文献
Cheung, Chi Wai; Surry, David S.; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 14 p. 3734 - 3737
反应条件
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine in dichloromethane T=20°C; 16 h;
参考文献
Aventis Pharma Deutschland GmbH
Patent: EP1479675 A1, 2004 ;
Location in patent: Page 62 ;
EP 1479675 A1
反应条件
1: Et3N / CH2Cl2 / 18 h / 20 °C 2: H2 / Pd/C / ethanol View Scheme
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
1: Et3N / CH2Cl2 / 18 h / 20 °C 2: H2 / Pd/C / ethanol View Scheme
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
in ethanol; water Heating;
参考文献
Husain, M. I.; Shukla, Sarveshwar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 761 - 764
反应条件
in ethanol; water
Heating;
参考文献
Husain, M. I.; Shukla, Sarveshwar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 761 - 764