2-烯丙基-1,4-二甲基苯合成路线 (共 15 条)
反应条件
in dichloromethane
0.5 h; Ambient temperature;
参考文献
Ochial; Fujita; Arimoto; Yamaguchi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 1 p. 86 - 93
反应条件
aluminum oxide; silica gel; potassium carbonate; zinc(II) chloride in 1,2-dichloro-ethane
T=30°C; 1 h;
参考文献
Kodomari, Mitsuo; Nawa, Satoru; Miyoshi, Tadahiro
Journal of the Chemical Society, Chemical Communications, 1995 , # 18 p. 1895 - 1896
反应条件
P(i-BuNCH2CH2)3N; cesium fluoride; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane
T=100 - 110°C; Stille reaction; Title compound not separated from byproducts;
参考文献
Su, Weiping; Urgaonkar, Sameer; Verkade, John G.
Organic Letters, 2004 , vol. 6, # 9 p. 1421 - 1424
反应条件
iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane
3 h; Ambient temperature;
参考文献
Lee, Kilsung; Kim, Dae Young; Oh, Dong Young
Tetrahedron Letters, 1988 , vol. 29, # 6 p. 667 - 668
反应条件
Pb3BrF5
T=60°C; 2 h;
参考文献
Ichihara, Junko
Chemical Communications, 1997 , # 19 p. 1921 - 1922
反应条件
1: aq. NaOH
2: (i) LiAlH4, (ii) TsOH
View Scheme
参考文献
Hansen,H.-J. et al.
Helvetica Chimica Acta, 1968 , vol. 51, p. 828 - 867
反应条件
(i) LiAlH4, (ii) TsOH; Multistep reaction;
参考文献
Hansen,H.-J. et al.
Helvetica Chimica Acta, 1968 , vol. 51, p. 828 - 867
反应条件
zinc(II) chloride
T=120°C; temperatures, ΔH(excit.), ΔS(excit); the energy of activation; the preexponential factor.; Rate constantProduct distributionKinetics;
参考文献
Magerramov, M. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 305 - 307
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 352 - 355
反应条件
zinc(II) chloride
T=120°C; 1.5 h; the competing reaction with p-xylene and naphthalene;; Rate constantProduct distribution;
参考文献
Magerramov, M. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 305 - 307
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 352 - 355
反应条件
zinc(II) chloride
T=120°C; 1.5 h; the competing reaction with p-xylene and α-methylnaphthalene;; Rate constantProduct distribution;
参考文献
Magerramov, M. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 305 - 307
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 352 - 355