二(1-苯并三唑基)甲硫酮合成路线 （共 20 条）
反应条件
1: aniline; Bt-CS-Bt in tetrahydrofuran
36 h;
2: pyrrolidine With triethylamine in tetrahydrofuran
36 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
1: triethylamine / dichloromethane / 0.08 h / 20 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.2 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
triethylamine in tetrahydrofuran
72 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
in dichloromethane
T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
in dichloromethane
T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
in dichloromethane
T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
in dichloromethane
T=20°C; 18 h;
参考文献
Katritzky, Alan R.; Ledoux, Stephane; Witek, Rachel M.; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 9 p. 2976 - 2982
反应条件
1: pyridine / dichloromethane / 0 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.25 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
1: triethylamine / dichloromethane / 0.2 h / 20 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.23 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
反应条件
1: pyridine / dichloromethane / 0 °C / |Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane / toluene / 0.33 h / 110 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Dhananjay; Mishra, Bhuwan B.; Tiwari, Vinod K.
Journal of Organic Chemistry, 2014 , vol. 79, # 1 p. 251 - 266
