1-(三甲基硅基)苯并三氮唑合成路线 （共 29 条）
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature
2: 90 percent / Ambient temperature
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
in dichloromethane; toluene
1 h; Ambient temperature;
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
参考文献
Gasparini, J. P.; Gassend, R.; Maire, J. C.; Elguero, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 141 - 150
反应条件
1: heptafluorobutyric acid chloride; 1-(trimethylsilanyl)-1H-benzotriazole in tetrahydrofuran
T=20°C; 3 h;
2: pyrrolidine T=20°C; 6 h;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
参考文献
Gasparini, J. P.; Gassend, R.; Maire, J. C.; Elguero, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 2 p. 141 - 150
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature
2: 95 percent / Ambient temperature
3: 82 percent / 120 °C
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature
2: 95 percent / Ambient temperature
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
1: heptafluorobutyric acid chloride; 1-(trimethylsilanyl)-1H-benzotriazole in tetrahydrofuran
T=20°C; 3 h;
2: 1-amino-1-phenylethane T=20°C; 6 h;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
参考文献
Katritzky, Alan R.; Shobana; Pernak, Juliusz; Afridi; Fan, Wei-Qiang
Tetrahedron, 1992 , vol. 48, # 37 p. 7817 - 7822
