1-乙氧基-2,2,2-三氟乙醇合成路线 （共 58 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane 24 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 93, # 2 p. 165 - 170
反应条件
aluminium trichloride in dichloromethane 2.5 h; Ambient temperatureother Lewis acids, other temperature, other times; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 93, # 2 p. 165 - 170
反应条件
zinc(II) iodide in 1,4-dioxane
参考文献
Kubota, Toshio; Iijima, Masahiro; Tanaka, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1351 - 1354
反应条件
5-[(2S)-pyrrolidine-2-yl]-1H-tetrazole in 1,2-dichloro-ethane T=40°C; Aldol condensation; 3 h; optical yield given as percent eestereoselective reaction;
参考文献
Funabiki, Kazumasa; Itoh, Yuya; Kubota, Yasuhiro; Matsui, Masaki
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3545 - 3550
反应条件
5A molecular sieve in 1,4-dioxane Substitution; 144 h;
参考文献
Ingrassia, Laurent; Mulliez, Michel
Synthesis, 1999 , # 10 p. 1731 - 1738
反应条件
L-proline in dimethyl sulfoxide T=20°C; 192 h; Product distribution / selectivity;
参考文献
US2005/119507 A1, ;
Page/Page column 4-5 ;
反应条件
1: in hexane T=0°C; 168 h; 2: With hydrogenchloride in hexane 3 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 18 p. 2056 - 2057
反应条件
1: in hexane T=20°C; 7 h; 2: With hydrogenchloride in hexane 3 h; Title compound not separated from byproducts;
参考文献
Chemical Communications, , # 18 p. 2056 - 2057
反应条件
potassium hydroxide in water 6 h; Heating;
参考文献
FUjii, Shozo; Maki, Yasuo; Kimoto, Hiroshi; Cohen, Louis A.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 581 - 590
参考文献
Bayer Aktiengesellschaft
Patent: US4808623 A1, 1989 ;
