1-对茴香基-1-苯基乙烯合成路线 （共 99 条）
反应条件
pentacarbonyl(η2-cis-cyclooctene)chromium(0) in dichloromethane
16 h; Ambient temperature;
参考文献
Pfeiffer, Juergen; Nieger, Martin; Doetz, Karl Heinz
European Journal of Organic Chemistry, 1998 , # 6 p. 1011 - 1022
反应条件
4-Methylpyridine; di-tert-butyl dicarbonate; lithium chloride; palladium dichloride in 1-methyl-pyrrolidin-2-one
T=120°C; Heck olefination; 16 h; Title compound not separated from byproducts;
参考文献
Goossen, Lukas J.; Paetzold, Jens; Winkel, Lars
Synlett, 2002 , # 10 p. 1721 - 1723
反应条件
1: tetrahydrofuran / 60 °C
2: H2SO4; acetic acid
View Scheme
参考文献
Xing, Dong; Guan, Bingtao; Cai, Guixin; Fang, Zhao; Yang, Liping; Shi, Zhangjie
Organic Letters, 2006 , vol. 8, # 4 p. 693 - 696
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran; diethyl ether
T=75°C; Kumada type cross-coupling reaction; 16 h; Inert atmosphere;
参考文献
Sabarre, Anthony; Love, Jennifer
Organic Letters, 2008 , vol. 10, # 18 p. 3941 - 3944
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(I) acetate; triethylamine in methanol
Suzuki-Miyaura reaction; 0.333333 h; Ultrasonic wawes;
参考文献
Singh, Fateh V.; Milagre, Humberto M.S.; Eberlin, Marcos N.; Stefani, Helio A.
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2312 - 2316
反应条件
potassium hydroxide; bis(dibenzylideneacetone)-palladium(0) in methanol
T=20°C; Inert atmosphere;
参考文献
Sore, Hannah F.; Boehner, Christine M.; Laraia, Luca; Logoteta, Patrizia; Prestinari, Cora; Scott, Matthew; Williams, Katharine; Galloway, Warren R. J. D.; Spring, David R.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 504 - 515
反应条件
1: (1,2-dibromo-ethyl)-benzene With potassium hydroxide in tetrahydrofuran
T=100°C; 1 h;
2: (4-methoxyphenyl)-boronic acid With palladium diacetate; triphenylphosphine in tetrahydrofuran; methanol
T=100°C; Suzuki coupling; 1 h;
参考文献
Lando, Vanusa R.; Monteiro, Adriano L.
Organic Letters, 2003 , vol. 5, # 16 p. 2891 - 2894
反应条件
sulfuric acid in acetonitrile
T=0°C; 0.0166667 h;
参考文献
Nakamura, Ryota; Obora, Yasushi; Ishii, Yasutaka
Chemical Communications, 2008 , # 29 p. 3417 - 3419
反应条件
trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate)
T=20°C; 24 h;
参考文献
Bhilare, Sachin V.; Darvatkar, Nitin B.; Deorukhkar, Amol R.; Raut, Dilip G.; Trivedi, Girish K.; Salunkhe, Manikrao M.
Tetrahedron Letters, 2009 , vol. 50, # 8 p. 893 - 896
反应条件
tetrakis(triphenylphosphine) palladium(0); oxygen; copper(l) chloride; lithium tert-butylate in 1,4-dioxane
T=70°C; 5 h;
参考文献
Zhao, Xia; Jing, Jing; Lu, Kui; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2010 , vol. 46, # 10 p. 1724 - 1726
