2,2,2-三氟苯乙酮合成路线 （共 295 条）
反应条件
aluminium trichloride in carbon disulfide T=-40°C; 3 h;
参考文献
Hull, William E.; Seeholzer, Klaus; Baumeister, Marlies; Ugi, Ivar
Tetrahedron, 1986 , vol. 42, # 2 p. 547 - 552
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; toluene 18 h; Ambient temperature;
参考文献
Wiedemann, Juergen; Heiner, Thomas; Mloston, Gregorz; Prakash, G.K. Surya; Olah, George A.
Angewandte Chemie - International Edition, 1998 , vol. 37, # 6 p. 820 - 821
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=-50 - -20°C;
参考文献
Prakash, G. K. Surya; Hu, Jinbo; Olah, George A.
Organic Letters, 2003 , vol. 5, # 18 p. 3253 - 3256
反应条件
[18F]fluorine; [18F]fluoride; fluorine in acetonitrile T=-45°C; 0.166667 h;
参考文献
University of Southern California
Patent: US6872855 B1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 5026 - 5030
参考文献
Aareskjold, Kare; Liaaen-Jensen, Synnove
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 8 p. 499 - 504
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in dichloromethane; acetonitrile T=-78 - 0°C; 2 h;
参考文献
Prakash, G.K. Surya; Hu, Jinbo; Alauddin, Mian M.; Conti, Peter S.; Olah, George A.
Journal of Fluorine Chemistry, 2003 , vol. 121, # 2 p. 239 - 243
反应条件
1: 86 percent / CH2Cl2 / 0 °C / Irradiation 2: H2O, B(OH)3 / ethanol / 8 h / 80 °C View Scheme
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.; Reibenspies
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8050 - 8059
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Creary, Xavier
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 5026 - 5030
反应条件
aluminium trichloride in carbon disulfide T=35 - 40°C; 45 h;
参考文献
Simchen, Gerhard; Schmidt, Andreas
Synthesis, 1996 , # 9 p. 1093 - 1094
