2,2,2-三氟苯乙酮合成路线 （共 295 条）
反应条件
n-butyllithium in hexane; toluene T=0°C; 16 h;
参考文献
Sokeirik, Yasser Samir; Sato, Kazuyuki; Omote, Masaaki; Ando, Akira; Kumadaki, Itsumaro
Tetrahedron Letters, 2006 , vol. 47, # 16 p. 2821 - 2824
反应条件
1: sodium tetrahydroborate / methanol / 0.75 h 2: Candida antarctica / toluene / 168 h / |Enzymatic reaction View Scheme
参考文献
Ribeiro, Sandra S.; Raminelli, Cristiano; Porto, Andre L.M.
Journal of Fluorine Chemistry, 2013 , vol. 154, p. 53 - 59
反应条件
in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Chong; Loewith
Synthetic Communications, 1993 , vol. 23, # 15 p. 2145 - 2150
反应条件
1: With lithium hexamethyldisilazane in tetrahydrofuran; toluene T=20°C; 0.25 h; 2: With sodium hydroxide; dimethylsulfide borane complex in tetrahydrofuran; toluene T=20°C; 1.5 h; 3: With hydrogenchloride in diethyl ether; toluene T=20°C; 1 h;
参考文献
Gosselin, Francis; O'Shea, Paul D.; Roy, Stephanie; Reamer, Robert A.; Chen, Cheng-Yi; Volante, Ralph P.
Organic Letters, 2005 , vol. 7, # 2 p. 355 - 358
反应条件
in acetonitrile T=23°C; Flash photolysis; Kinetics;
参考文献
Lathioor, Edward C.; Leigh, William J.
Photochemistry and Photobiology, 2006 , vol. 82, # 1 p. 291 - 300
反应条件
sulfur(IV) fluoride T=100°C; 8 h;
参考文献
Dreher, Bernhard; Prescher, Dietrich; Dmowski, Wojciech; Wozniacki, Ryszard
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 118
反应条件
phosphorus pentachloride T=175°C;
参考文献
Eliseenkov,E.V. et al.
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 781 - 785,721 - 724
参考文献
Cohen; Wolosinski; Scheuer
Journal of the American Chemical Society, 1949 , vol. 71, p. 3439
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Simons; Ramler
Journal of the American Chemical Society, 1943 , vol. 65, p. 389,390
反应条件
Irradiation; Quantum yieldMechanism;
参考文献
Wagner, Peter J.; Truman, Royal J.; Scaiano, J. C.
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7093 - 7097
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Jablonski, Lukas; Billard, Thierry; Langlois, Bernard R.
Tetrahedron Letters, 2003 , vol. 44, # 5 p. 1055 - 1057
