2-甲基-6-硝基苯甲酸酐合成路线 (共 11 条)
反应条件
1: With thionyl chloride in dichloromethane T=20°C; 15 h; 2: 6-methyl-2-nitrobenzoic acid With pyridine in dichloromethane T=20°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 43, # 42 p. 7535 - 7539
反应条件
pyridine T=20°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 6 p. 1822 - 1830
反应条件
triethylamine in chloroform-d1 T=20°C; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 69, # 6 p. 1822 - 1830
参考文献
Chemische Berichte, , vol. 52, p. 1083
反应条件
1: sulfuric acid 2: potassium nitrite; sulfuric acid 3: thionyl chloride 4: diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 52, p. 1083
反应条件
1: potassium nitrite; sulfuric acid 2: thionyl chloride 3: diethyl ether View Scheme
参考文献
Chemische Berichte, , vol. 52, p. 1083
反应条件
triethylamine in chloroform-d1 T=20°C; Title compound not separated from byproducts;
参考文献
Shiina, Isamu; Kubota, Mari; Oshiumi, Hiromi; Hashizume, Minako
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1822 - 1830
反应条件
4-(N,N-dimethlyamino)pyridine; 2-azidoethanol in dichloromethane T=20°C;
参考文献
Shiina, Isamu; Ibuka, Ryoutarou; Kubota, Mari
Chemistry Letters, 2002 , # 3 p. 286 - 287
反应条件
4-(N,N-dimethlyamino)pyridine; 2-azidoethanol in dichloromethane
T=20°C;
参考文献
Shiina, Isamu; Ibuka, Ryoutarou; Kubota, Mari
Chemistry Letters, 2002 , # 3 p. 286 - 287
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=20°C; 20 h;
参考文献
Shiina, Isamu; Kubota, Mari; Oshiumi, Hiromi; Hashizume, Minako
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1822 - 1830