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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻碘苯腈
合成路线
（共 54 条）
4387-36-4
邻碘苯腈
→
反应条件
39959-51-8
2-碘苄胺
反应条件
1: With borane-THF in tetrahydrofuran T=0 - 20°C; 24 h; Inert atmosphere; 2: With sodium hydroxide in water pH=Ca. 10;
参考文献
Shao, Changzhun; Stolte, Matthias; Wuerthner, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 29 p. 7482 - 7486
Angew. Chem., 2013 , vol. 125, # 29 p. 7630 - 7634,5
6213-94-1
乙烯氧基三甲基硅烷
+
4387-36-4
邻碘苯腈
→
反应条件
91054-33-0
2-乙酰苯甲腈
反应条件
palladium diacetate; triethylamine; triphenylphosphine in dimethyl sulfoxide; N,N-dimethyl-formamide T=20 - 100°C; Heck Reaction; 2 h; Microwave irradiation; regioselective reaction;
参考文献
Qian, Wangke; Zhang, Lei; Sun, Haifeng; Jiang, Hualiang; Liu, Hong
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 17 p. 3231 - 3236
4387-36-4
邻碘苯腈
+
501-65-5
二苯基乙炔
→
反应条件
1801-42-9
2,3-二苯基-1-二氢茚酮
反应条件
water; triethylamine; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=130°C; 24 h;
参考文献
Pletnev, Alexandre A.; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9276 - 9287
4387-36-4
邻碘苯腈
→
反应条件
938-16-9
2,2,2-三甲基苯乙酮
反应条件
1.1: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 24 h / 135 °C / |Inert atmosphere; |Sealed tube 2.1: methyllithium / tetrahydrofuran; diethyl ether; pentane / 20 h / 0 - 20 °C / |Inert atmosphere 2.2: 1 h / 20 °C / |Inert atmosphere 3.1: ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride / para-xylene / 24 h / 140 °C / |Schlenk technique; |Glovebox; |Inert atmosphere View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 741-742, # 1 p. 148 - 152
4387-36-4
邻碘苯腈
→
反应条件
938-16-9
2,2,2-三甲基苯乙酮
+
1448622-36-3
反应条件
1.1: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 24 h / 135 °C / |Inert atmosphere; |Sealed tube 2.1: methyllithium / tetrahydrofuran; diethyl ether; pentane / 20 h / 0 - 20 °C / |Inert atmosphere 2.2: 1 h / 20 °C / |Inert atmosphere 3.1: ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride / para-xylene / 24 h / 140 °C / |Schlenk technique; |Glovebox; |Inert atmosphere View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 741-742, # 1 p. 148 - 152
4387-36-4
邻碘苯腈
→
反应条件
938-16-9
2,2,2-三甲基苯乙酮
+
1448622-37-4
反应条件
1.1: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 24 h / 135 °C / |Inert atmosphere; |Sealed tube 2.1: methyllithium / tetrahydrofuran; diethyl ether; pentane / 20 h / 0 - 20 °C / |Inert atmosphere 2.2: 1 h / 20 °C / |Inert atmosphere 3.1: ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride / para-xylene / 24 h / 140 °C / |Schlenk technique; |Glovebox; |Inert atmosphere View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 741-742, # 1 p. 148 - 152
344-04-7
+
4387-36-4
邻碘苯腈
→
反应条件
4341-02-0
+
434-90-2
反应条件
copper T=190 - 200°C; 18 h;
参考文献
Frohn, H. J.; Klose, A.; Bardin, V. V.
Journal of Fluorine Chemistry, 1993 , vol. 64, # 3 p. 201 - 216
4387-36-4
邻碘苯腈
→
反应条件
611-20-1
反应条件
1.1: copper(l) iodide; 1,10-phenanthroline; caesium carbonate / toluene / 14 h / 110 °C / Inert atmosphere; Sealed tube 2.1: cesium fluoride / N,N-dimethyl-formamide / 1 h / 60 °C / Inert atmosphere 2.2: Inert atmosphere View Scheme
参考文献
Dibakar, Mullick; Prakash, Anjanappa; Selvakumar, Kumaravel; Ruckmani, Kandasamy; Sivakumar, Manickam
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5338 - 5341
4387-36-4
邻碘苯腈
+
1137728-03-0
→
反应条件
23973-65-1
反应条件
1: C5H12IO3PZn With [RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,1'-bis(diphenylphosphino)ferrocene in tetrahydrofuran 0.0833333 h; Inert atmosphere; 2: 2-iodobenzonitrile in tetrahydrofuran T=60°C; Negishi coupling reaction; 10 h; Inert atmosphere;
参考文献
Takahashi, Hideki; Inagaki, Shinya; Yoshii, Naoko; Gao, Fuxing; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2794 - 2797
4387-36-4
邻碘苯腈
→
反应条件
1885-29-6
反应条件
ammonium hydroxide; potassium phosphate; copper ferrite T=100°C; 12 h; Sealed tube; chemoselective reaction;
参考文献
Kumar, A. Suresh; Ramani; Sreedhar
Synlett, 2013 , vol. 24, # 8 art. no. ST-2013-D0032-L, p. 938 - 942
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