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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
439-03-2
合成路线
(共 43 条)
145259-92-3
+
439-03-2
→
反应条件
反应条件
boron trifluoride diethyl etherate in dichloromethane 62 h; Ambient temperature;
参考文献
Ziegler, Thomas; Eckhardt, E.; Pantkowski, G.
Journal of Carbohydrate Chemistry, 1994 , vol. 13, # 1 p. 81 - 110
145259-93-4
+
439-03-2
→
反应条件
13992-16-0
反应条件
boron trifluoride diethyl etherate in dichloromethane 20 h; Ambient temperature;
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 1 p. 81 - 110
108-98-5
硫酚
+
439-03-2
→
反应条件
13992-16-0
反应条件
diethyl ether; boron trifluoride in dichloromethane T=25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nicolaou; Chucholowski; Dolle; Randall
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 17, p. 1155 - 1156
439-03-2
→
反应条件
3482-57-3
4-硝基苯基-β-D-纤维二糖苷
反应条件
1: methanol; sodium methylate / 20 °C 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
150-76-5
4-甲氧基苯酚
+
439-03-2
→
反应条件
2872-65-3
对甲氧基苯基 2,3,4,6-O-四乙酰基-beta-D-吡喃半乳糖苷
反应条件
2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate in dichloromethane T=20°C; Etherification; 1 h;
参考文献
Oyama, Kin-Ichi; Kondo, Tadao
Synlett, 1999 , # 10 p. 1627 - 1629
150-76-5
4-甲氧基苯酚
+
439-03-2
→
反应条件
2872-65-3
对甲氧基苯基 2,3,4,6-O-四乙酰基-beta-D-吡喃半乳糖苷
+
84380-06-3
反应条件
boron trifluoride diethyl etherate in acetonitrile 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Yamaguchi, Masahiko; Horiguchi, Akira; Fukuda, Akira; Minami, Toru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 4 p. 1079 - 1082
439-03-2
→
反应条件
4419-94-7
4-硝基苯基-Β-D-乳糖苷
反应条件
1: methanol; sodium methylate / 20 °C 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
145259-93-4
+
439-03-2
→
反应条件
13992-16-0
反应条件
boron trifluoride diethyl etherate in dichloromethane 20 h; Ambient temperature;
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 1 p. 81 - 110
108-98-5
硫酚
+
439-03-2
→
反应条件
13992-16-0
反应条件
diethyl ether; boron trifluoride in dichloromethane T=25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nicolaou; Chucholowski; Dolle; Randall
Journal of the Chemical Society - Series Chemical Communications, 1984 , vol. NO. 17, p. 1155 - 1156
150-76-5
4-甲氧基苯酚
+
439-03-2
→
反应条件
2872-65-3
对甲氧基苯基 2,3,4,6-O-四乙酰基-beta-D-吡喃半乳糖苷
反应条件
2,6-di-tert-butyl-4-methylpyridine; boron trifluoride diethyl etherate in dichloromethane T=20°C; Etherification; 1 h;
参考文献
Oyama, Kin-Ichi; Kondo, Tadao
Synlett, 1999 , # 10 p. 1627 - 1629
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