1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 4-hydroxybutanol; N-[(1S,2S)-2-amino-1,2-diphenylethyl]-p-tolylsulphonamide; potassium hydroxide T=110°C; 72 h; optical yield given as percent ee;
参考文献
Chemistry - An Asian Journal, , vol. 5, # 3 p. 538 - 542
反应条件
2: Raney nickel; diethyl ether / Hydrogenation View Scheme
参考文献
Journal of the Chemical Society, , p. 1697,1700
反应条件
oxygen; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=50°C; 24 h;
参考文献
Gade, Narendar Reddy; Devendram; Pal, Manojit; Iqbal, Javed
Chemical Communications, 2013 , vol. 49, # 72 p. 7926 - 7928
反应条件
[O3ReOSiPh3] in diethyl ether T=0°C; 0.5 h;
参考文献
Morrill, Christie; Grubbs, Robert H.
Journal of the American Chemical Society, 2005 , vol. 127, # 9 p. 2842 - 2843
参考文献
Burton; Ingold
Journal of the Chemical Society, 1928 , p. 915
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran; toluene T=35 - 100°C; 15 h; Inert atmosphere; diastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
hydrogen bromide; antimony(III)tribromide in diethyl ether
参考文献
Ouellette,R.J. et al.
Journal of the American Chemical Society, 1968 , vol. 90, p. 1619 - 1624
反应条件
1: With Grubb's 2nd generation catalyst in toluene T=110°C; 0.5 h; Inert atmosphere; 2: With sodium hydroxide in toluene T=130°C; 3 h; Reagent/catalyst;
参考文献
Schmidt, Bernd; Hauke, Sylvia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 25 p. 4194 - 4206
反应条件
lithium aluminium tetrahydride; bis(cyclopentadienyl)titanium dichloride 1.) THF, -20 deg C, 3 h, -> r.t., overnight; 2.) hydrolysis; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sato, Fumie; Tomuro, Yasuji; Ishikawa, Hiroaki; Oikawa, Takeshi
Chemistry Letters, 1980 , p. 103 - 106
参考文献
Klages
Chemische Berichte, 1906 , vol. 39, p. 2589
